D21.03 - Chemical and Physical Testing

SIGNIFICANCE AND USE
3.1 This test method is used to determine the effect of freezing on floor polishes. It may be used to predict the stability of a floor polish when exposed to freezing.
SCOPE
1.1 This test method covers the determination of the stability of polymer emulsion floor polishes when these are exposed to repeated cycles of freezing and thawing. Possible degradation of the emulsion is observed and possible reduction of initial gloss is measured.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
2.1 This test method is generally accepted for the preparation of floor polish and floor polish polymers for the analysis of total zinc content. Knowing the total zinc content of a floor finish or polymer can aid in determining the proper disposal method of used or unwanted product.
SCOPE
1.1 This laboratory test method covers the analysis of floor polishes and floor polish polymers for total zinc content.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 This test method is used to determine the effect of freezing on wax emulsion floor polishes. It may be used to predict the stability of a floor polish in transit or when exposed to freezing, and whether or not the polish is damaged by freezing.
SCOPE
1.1 This test method covers the determination of the stability of wax emulsion floor polishes when these are exposed to repeated cycles of freezing and thawing. Possible degradation of the emulsion is observed and possible reduction of initial gloss is measured.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 This test method is not absolute but does give an indication of the useful shelf-life of a liquid water-emulsion floor polish. Will indicate whether a polish will gel or remain a usable liquid over the desired storage life of the product. It should be noted that polishes of different composition types will vary in useful storage life under identical storage conditions.
SCOPE
1.1 This test method covers the storage stability of liquid water-emulsion floor polishes.  
1.2 Storage for 30 days at 52 °C (125 °F), while not a guarantee of one year stability at 21 °C (70 °F), is believed to be a more reliable indicator of storage stability than similar tests of shorter duration.  
Note 1: The 60° specular gloss on black glass determined by Test Method D1455, may be used to confirm this observation. A substantial difference in gloss between aged and unaged samples is an indication of instability. A shelf stability of one year can be reasonably expected of the material in question if duplicate samples remain unchanged for 30 days at 52 °C ± 1.1 °C (125 °F ± 2 °F). If one or both duplicates show more than slight viscosity increases or slight creaming, other evidence of stability must be sought.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
2.1 Nonvolatile matter determination is useful as a quality control test, when used in conjunction with other tests, to assure specification compliance.
SCOPE
1.1 This test method covers the determination of nonvolatile matter (total solids) in a water-emulsion, organic solvent-based liquid and paste floor polishes, and polymer-emulsion-type floor polishes.  
1.2 This test method recognizes that the products may contain material that will slowly volatilize or change chemically with a resulting change in weight of the nonvolatile matter. Therefore, since drying to constant weight is impractical, specific drying times have been selected.  
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 This test method determines the amount of sediment in water-emulsion polishes. Sediment is generally believed to have negative effects on water-emulsion polish properties.
SCOPE
1.1 This test method covers the determination of sediment in water-emulsion polishes by means of a centrifuge.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 The laboratory technique described in this test method is used to evaluate the clarity and yellowness of water-based “clear” floor polishes for product development or quality control purposes.
SCOPE
1.1 This test method covers measurement of the degree of clarity and depth of yellowness of water-based clear floor polishes.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 The purpose of this test is not to fully identify and characterize a polymer, but to identify a variety of basic parameters needed to predetermine the usefulness of the polymer in formulations as well as for Quality Control purposes.  
3.2 A statement of precision and accuracy is not appropriate in this case.
SCOPE
1.1 These test methods cover test procedures for emulsion polymers that are used in water-based floor polishes. The term “emulsion polymers” is used primarily to denote those materials produced by regular emulsion polymerization techniques, but may be extended to those polymers that are subsequently emulsified or dispersed after polymerization. Unless otherwise noted, the tests may be used for any polymer or copolymer systems. The methods appear in the following order:    
Section  
Sampling  
4  
Total Solids  
5  
pH Value  
6  
Apparent Viscosity  
7  
Sediment  
8  
Storage Stability  
9  
Freeze-thaw Stability  
10  
Specific Gravity  
11  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 Solids (nonvolatile matter) determinations of polishes, resin solutions, and wax emulsions take 2 to 4 h in accordance with Test Method D2834, not counting preparation time.  
4.2 Curves of solids/refractive index provide a means for determining solids in a matter of minutes.  
4.3 This practice is particularly useful for quality control and in process control for the production of polishes and polish components.
SCOPE
1.1 This practice covers the use of a refractometer for determining the nonvolatile matter (total solids) in floor polishes. This practice is also applicable to resin solutions and wax emulsions used in floor polishes.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 This test method is used to determine the effect of freezing on wax emulsion floor polishes. It may be used to predict the stability of a floor polish in transit or when exposed to freezing, and whether or not the polish is damaged by freezing.
SCOPE
1.1 This test method covers the determination of the stability of wax emulsion floor polishes when these are exposed to repeated cycles of freezing and thawing. Possible degradation of the emulsion is observed and possible reduction of initial gloss is measured.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 The laboratory technique described in this test method is used to evaluate the clarity and yellowness of water-based “clear” floor polishes for product development or quality control purposes.
SCOPE
1.1 This test method covers measurement of the degree of clarity and depth of yellowness of water-based clear floor polishes.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
2.1 This test method is generally accepted for the preparation of floor polish and floor polish polymers for the analysis of total zinc content. Knowing the total zinc content of a floor finish or polymer can aid in determining the proper disposal method of used or unwanted product.
SCOPE
1.1 This laboratory test method covers the analysis of floor polishes and floor polish polymers for total zinc content.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
3.1 This test method is used to determine the effect of freezing on wax emulsion floor polishes. It may be used to predict the stability of a floor polish in transit or when exposed to freezing, and whether or not the polish is damaged by freezing.
SCOPE
1.1 This test method covers the determination of the stability of wax emulsion floor polishes when these are exposed to repeated cycles of freezing and thawing. Possible degradation of the emulsion is observed and possible reduction of initial gloss is measured.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
3.1 This test method determines the amount of sediment in water-emulsion polishes. Sediment is generally believed to have negative effects on water-emulsion polish properties.
SCOPE
1.1 This test method covers the determination of sediment in water-emulsion polishes by means of a centrifuge.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
2.1 Nonvolatile matter determination is useful as a quality control test, when used in conjunction with other tests, to assure specification compliance.
SCOPE
1.1 This test method covers the determination of nonvolatile matter (total solids) in a water-emulsion, organic solvent-based liquid and paste floor polishes, and polymer-emulsion-type floor polishes.  
1.2 This test method recognizes that the products may contain material that will slowly volatilize or change chemically with a resulting change in weight of the nonvolatile matter. Therefore, since drying to constant weight is impractical, specific drying times have been selected.  
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
3.1 This test method is not absolute but does give an indication of the useful shelf-life of a liquid water-emulsion floor polish. Will indicate whether a polish will gel or remain a usable liquid over the desired storage life of the product. It should be noted that polishes of different composition types will vary in useful storage life under identical storage conditions.
SCOPE
1.1 This test method covers the storage stability of liquid water-emulsion floor polishes.  
1.2 Storage for 30 days at 52°C (125°F), while not a guarantee of one year stability at 21°C (70°F), is believed to be a more reliable indicator of storage stability than similar tests of shorter duration.  
Note 1: The 60° specular gloss on black glass determined by Test Method D1455, may be used to confirm this observation. A substantial difference in gloss between aged and unaged samples is an indication of instability. A shelf stability of one year can be reasonably expected of the material in question if duplicate samples remain unchanged for 30 days at 52 ± 1.1°C (125 ± 2°F). If one or both duplicates show more than slight viscosity increases or slight creaming, other evidence of stability must be sought.  
1.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
3.1 This test method is used to determine the effect of freezing on floor polishes. It may be used to predict the stability of a floor polish when exposed to freezing.
SCOPE
1.1 This test method covers the determination of the stability of polymer emulsion floor polishes when these are exposed to repeated cycles of freezing and thawing. Possible degradation of the emulsion is observed and possible reduction of initial gloss is measured.  
1.2 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
3.1 The purpose of this test is not to fully identify and characterize a polymer, but to identify a variety of basic parameters needed to predetermine the usefulness of the polymer in formulations as well as for Quality Control purposes.  
3.2 A statement of precision and accuracy is not appropriate in this case.
SCOPE
1.1 These test methods cover test procedures for emulsion polymers that are used in water-based floor polishes. The term “emulsion polymers” is used primarily to denote those materials produced by regular emulsion polymerization techniques, but may be extended to those polymers that are subsequently emulsified or dispersed after polymerization. Unless otherwise noted, the tests may be used for any polymer or copolymer systems. The methods appear in the following order:    
Section  
Sampling  
4  
Total Solids  
5  
pH Value  
6  
Apparent Viscosity  
7  
Sediment  
8  
Storage Stability  
9  
Freeze-thaw Stability  
10  
Specific Gravity  
11  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
4.1 Solids (nonvolatile matter) determinations of polishes, resin solutions, and wax emulsions take 2 to 4 h in accordance with Test Method D2834, not counting preparation time.  
4.2 Curves of solids/refractive index provide a means for determining solids in a matter of minutes.  
4.3 This practice is particularly useful for quality control and in process control for the production of polishes and polish components.
SCOPE
1.1 This practice covers the use of a refractometer for determining the nonvolatile matter (total solids) in floor polishes. This practice is also applicable to resin solutions and wax emulsions used in floor polishes.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
The laboratory technique described in this test method is used to evaluate the clarity and yellowness of water-based “clear” floor polishes for product development or quality control purposes.
SCOPE
1.1 This test method covers measurement of the degree of clarity and depth of yellowness of water-based clear floor polishes.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
This test method is not absolute but does give an indication of the useful shelf-life of a liquid water-emulsion floor polish. Will indicate whether a polish will gel or remain a usable liquid over the desired storage life of the product. It should be noted that polishes of different composition types will vary in useful storage life under identical storage conditions.
SCOPE
1.1 This test method covers the storage stability of liquid water-emulsion floor polishes.
1.2 Storage for 30 days at 52°C (125°F), while not a guarantee of one year stability at 21°C (70°F), is believed to be a more reliable indicator of storage stability than similar tests of shorter duration.
Note 1—The 60° specular gloss on black glass determined by Test Method D 1455, may be used to confirm this observation. A substantial difference in gloss between aged and unaged samples is an indication of instability. A shelf stability of one year can be reasonably expected of the material in question if duplicate samples remain unchanged for 30 days at 52 ± 1.1°C (125 ± 2°F). If one or both duplicates show more than slight viscosity increases or slight creaming, other evidence of stability must be sought.  
1.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
This test method is used to determine the effect of freezing on wax emulsion floor polishes. It may be used to predict the stability of a floor polish in transit or when exposed to freezing, and whether or not the polish is damaged by freezing.
SCOPE
1.1 This test method covers the determination of the stability of wax emulsion floor polishes when these are exposed to repeated cycles of freezing and thawing. Possible degradation of the emulsion is observed and possible reduction of initial gloss is measured.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
Nonvolatile matter determination is useful as a quality control test, when used in conjunction with other tests, to assure specification compliance.
SCOPE
1.1 This test method covers the determination of nonvolatile matter (total solids) in a water-emulsion, organic solvent-based liquid and paste floor polishes, and polymer-emulsion-type floor polishes.
1.2 This test method recognizes that the products may contain material that will slowly volatilize or change chemically with a resulting change in weight of the nonvolatile matter. Therefore, since drying to constant weight is impractical, specific drying times have been selected.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
This test method determines the amount of sediment in water-emulsion polishes. Sediment is generally believed to have negative effects on water-emulsion polish properties.
SCOPE
^SCOPE:
1.1 This test method covers the determination of sediment in water-emulsion polishes by means of a centrifuge.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
This test method is generally accepted for the preparation of floor polish and floor polish polymers for the analysis of total zinc content. Knowing the total zinc content of a floor finish or polymer can aid in determining the proper disposal method of used or unwanted product.
SCOPE
1.1 This laboratory test method covers the analysis of floor polishes and floor polish polymers for total zinc content.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
Solids (nonvolatile matter) determinations of polishes, resin solutions, and wax emulsions take 2 to 4 h in accordance with Test Method D 2834, not counting preparation time.
Curves of solids/refractive index provide a means for determining solids in a matter of minutes.
This practice is particularly useful for quality control and in process control for the production of polishes and polish components.
SCOPE
1.1 This practice covers the use of a refractometer for determining the nonvolatile matter (total solids) in floor polishes. This practice is also applicable to resin solutions and wax emulsions used in floor polishes.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
>The purpose of this test is not to fully identify and characterize a polymer, but to identify a variety of basic parameters needed to predetermine the usefulness of the polymer in formulations as well as for Quality Control purposes.
A statement of precision and accuracy is not appropriate in this case.
SCOPE
1.1 These test methods cover test procedures for emulsion polymers that are used in water-based floor polishes. The term “emulsion polymers” is used primarily to denote those materials produced by regular emulsion polymerization techniques, but may be extended to those polymers that are subsequently emulsified or dispersed after polymerization. Unless otherwise noted, the tests may be used for any polymer or copolymer systems. The methods appear in the following order:
Section    Sampling4 Total Solids5 pH Value6 Apparent Viscosity7 Sediment8 Storage Stability9 Freeze-thaw Stability10 Specific Gravity11
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
This test method is used to determine the effect of freezing on floor polishes. It may be used to predict the stability of a floor polish when exposed to freezing.
SCOPE
1.1 This test method covers the determination of the stability of polymer emulsion floor polishes when these are exposed to repeated cycles of freezing and thawing. Possible degradation of the emulsion is observed and possible reduction of initial gloss is measured.
1.2 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
The purpose of this test is not to fully identify and characterize a polymer, but to identify a variety of basic parameters needed to predetermine the usefulness of the polymer in formulations as well as for Quality Control purposes.
A statement of precision and accuracy is not appropriate in this case.
SCOPE
1.1 These test methods cover test procedures for emulsion polymers that are used in water-based floor polishes. The term "emulsion polymers" is used primarily to denote those materials produced by regular emulsion polymerization techniques, but may be extended to those polymers that are subsequently emulsified or dispersed after polymerization. Unless otherwise noted, the tests may be used for any polymer or copolymer systems. The methods appear in the following order:SectionSamplingTotal SolidspH ValueApparent ViscositySedimentStorage StabilityFreeze-thaw StabilitySpecific Gravity
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
This test method is not absolute but does give an indication of the useful shelf-life of a liquid water-emulsion floor polish. Will indicate whether a polish will gel or remain a usable liquid over the desired storage life of the product. It should be noted that polishes of different composition types will vary in useful storage life under identical storage conditions.
SCOPE
1.1 This test method covers the storage stability of liquid water-emulsion floor polishes.
1.2 Storage for 30 days at 52°C (125°F), while not a guarantee of one year stability at 21°C (70°F), is believed to be a more reliable indicator of storage stability than similar tests of shorter duration.
Note 1—The 60 specular gloss on black glass determined by Test Method D 1455, may be used to confirm this observation. A substantial difference in gloss between aged and unaged samples is an indication of instability. A shelf stability of one year can be reasonably expected of the material in question if duplicate samples remain unchanged for 30 days at 52 1.1°C (125 2°F). If one or both duplicates show more than slight viscosity increases or slight creaming, other evidence of stability must be sought.1.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
This test method is used to determine the effect of freezing on floor polishes. It may be used to predict the stability of a floor polish when exposed to freezing.
SCOPE
1.1 This test method covers the determination of the stability of polymer emulsion floor polishes when these are exposed to repeated cycles of freezing and thawing. Possible degradation of the emulsion is observed and possible reduction of initial gloss is measured.
1.2 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
This test method is generally accepted for the preparation of floor polish and floor polish polymers for the analysis of total zinc content. Knowing the total zinc content of a floor finish or polymer can aid in determining the proper disposal method of used or unwanted product.
SCOPE
1.1 This laboratory test method covers the analysis of floor polishes and floor polish polymers for total zinc content.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SCOPE
1.1 These test methods cover test procedures for emulsion polymers that are used in water-based floor polishes. The term "emulsion polymers" is used primarily to denote those materials produced by regular emulsion polymerization techniques, but may be extended to those polymers that are subsequently emulsified or dispersed after polymerization. Unless otherwise noted, the tests may be used for any polymer or copolymer systems. The methods appear in the following order:  Section Sampling 4 Total solids 5 pH value 6 Apparent viscosity 7 Sediment 8 Storage stability 9 Freeze-thaw stability 10 Specific gravity 11
1.2 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SCOPE
1.1 This test method covers the determination of the stability of polymer emulsion floor polishes when these are exposed to repeated cycles of freezing and thawing. Possible degradation of the emulsion is observed and possible reduction of initial gloss is measured.  
1.2 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SCOPE
1.1 This test method covers the storage stability of liquid water-emulsion floor polishes.  
1.2 Storage for 30 days at 52°C (125°F), while not a guarantee of one year stability at 21°C (70°F), is believed to be a more reliable indicator of storage stability than similar tests of shorter duration.  Note-The 60° specular gloss on black glass determined by Test Method D1455, may be used to confirm this observation. A substantial difference in gloss between aged and unaged samples is an indication of instability. A shelf stability of one year can be reasonably expected of the material in question if duplicate samples remain unchanged for 30 days at 52 + 1.1°C (125 + 2°F). If one or both duplicates show more than slight viscosity increases or slight creaming, other evidence of stability must be sought.
1.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SCOPE
1.1 This practice covers the use of a refractometer for determining the nonvolatile matter (total solids) in floor polishes. This practice is also applicable to resin solutions and wax emulsions used in floor polishes.  
1.2 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
Solids (nonvolatile matter) determinations of polishes, resin solutions, and wax emulsions take 2 to 4 h in accordance with Test Method D 2834, not counting preparation time.
Curves of solids/refractive index provide a means for determining solids in a matter of minutes.
This practice is particularly useful for quality control and in process control for the production of polishes and polish components.
SCOPE
1.1 This practice covers the use of a refractometer for determining the nonvolatile matter (total solids) in floor polishes. This practice is also applicable to resin solutions and wax emulsions used in floor polishes.  
1.2 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
This test method determines the amount of sediment in water-emulsion polishes. Sediment is generally believed to have negative effects on water-emulsion polish properties.
SCOPE
1.1 This test method covers the determination of sediment in water-emulsion polishes by means of a centrifuge.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
Nonvolatile matter determination is useful as a quality control test, when used in conjunction with other tests, to assure specification compliance.
SCOPE
1.1 This test method covers the determination of nonvolatile matter (total solids) in a water-emulsion, organic solvent- base liquid and paste floor polishes, and polymer-emulsion-type floor polishes.  
1.2 This test method recognizes that the products may contain material that will slowly volatilize or change chemically with a resulting change in weight of the nonvolatile matter. Therefore, since drying to constant weight is impractical, specific drying times have been selected.  
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SCOPE
1.1 This test method covers the determination of nonvolatile matter (total solids) in a water-emulsion, organic solvent- base liquid and paste floor polishes, and polymer-emulsion-type floor polishes.  
1.2 This test method recognizes that the products may contain material that will slowly volatilize or change chemically with a resulting change in weight of the nonvolatile matter. Therefore, since drying to constant weight is impractical, specific drying times have been selected.  
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SCOPE
1.1 This test method covers the determination of nonvolatile matter (total solids) in a water-emulsion, organic solvent- base liquid and paste floor polishes, and polymer-emulsion-type floor polishes.  
1.2 This test method recognizes that the products may contain material that will slowly volatilize or change chemically with a resulting change in weight of the nonvolatile matter. Therefore, since drying to constant weight is impractical, specific drying times have been selected.  
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
The laboratory technique described in this test method is used to evaluate the clarity and yellowness of water-based “clear” floor polishes for product development or quality control purposes.
SCOPE
1.1 This test method covers measurement of the degree of clarity and depth of yellowness of water-based clear floor polishes.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
This test method is used to determine the effect of freezing on wax emulsion floor polishes. It may be used to predict the stability of a floor polish in transit or when exposed to freezing, and whether or not the polish is damaged by freezing.
SCOPE
1.1 This test method covers the determination of the stability of wax emulsion floor polishes when these are exposed to repeated cycles of freezing and thawing. Possible degradation of the emulsion is observed and possible reduction of initial gloss is measured.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SCOPE
1.1 This test method covers the determination of the stability of wax emulsion floor polishes when these are exposed to repeated cycles of freezing and thawing. Possible degradation of the emulsion is observed and possible reduction of initial gloss is measured.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SCOPE
1.1 This test method covers the determination of sediment in water-emulsion polishes by means of a centrifuge.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SCOPE
1.1 This test method covers measurement of the degree of clarity and depth of yellowness of water-based clear floor polishes.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.