71.040 - Analytical chemistry
ICS 71.040 Details
Analytical chemistry
Analytische Chemie
Chimie analytique
Analitska kemija
General Information
Frequently Asked Questions
ICS 71.040 is a classification code in the International Classification for Standards (ICS) system. It covers "Analytical chemistry". The ICS is a hierarchical classification system used to organize international, regional, and national standards, facilitating the search and identification of standards across different fields.
There are 3351 standards classified under ICS 71.040 (Analytical chemistry). These standards are published by international and regional standardization bodies including ISO, IEC, CEN, CENELEC, and ETSI.
The International Classification for Standards (ICS) is a hierarchical classification system maintained by ISO to organize standards and related documents. It uses a three-level structure with field (2 digits), group (3 digits), and sub-group (2 digits) codes. The ICS helps users find standards by subject area and enables statistical analysis of standards development activities.
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This document specifies a method for the determination of the time-weighted average mass concentration of soluble particulate fluorides and hydrofluoric acid (HF) in workplace air by collection of the particulate fluorides on a pre-filter and HF on an alkali-impregnated filter and analysis by ion chromatography.
This method is only applicable to determination of particulate fluorides that are soluble using the sample preparation procedure specified.
For aerosol sampling, this method is applicable to the personal sampling of the inhalable fraction of airborne particles, as defined in ISO 7708, and to static (area) sampling.
The method is applicable to the determination of masses of 0,005 mg to at least 1,25 mg of particulate fluorides per sample and 0,015 mg to at least 1,2 mg of HF per sample.
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This document specifies a test method for the sampling and analysis of airborne organic isocyanate (NCO) compounds in workplace air. The method covers organic compounds containing free isocyanate functional groups, including monomeric, oligomeric, prepolymeric and polymeric isocyanates, and addresses the measurement of total isocyanate groups in air samples collected for the assessment of occupational exposure.
The method is suitable for personal air sampling in the breathing zone for the determination of time-weighted average concentrations over sampling periods ranging from approximately 10 min to 8 h, although it can be applied to shorter sampling periods with high isocyanate air levels. It can also be used for background or fixed-location air sampling; however, due to aerodynamic effects, samplers designed for personal sampling do not necessarily exhibit the same collection characteristics when used for other purposes. It covers the measurement of airborne organic isocyanates over a concentration range of approximately 0,1 μg/m3 to 140 μg/m3 for a nominal air sample volume of 15 l; under the conditions specified in this document, typical qualitative and quantitative detection limits correspond to approximately 0,07 μg/m3 a nd 0 ,3 μg/m3, respectively, for a 15 l air sample.
This document does not apply to the simultaneous determination of isocyanates and amines, nor to modified methods employing alternative sampling devices or detection techniques not described in this document.
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This document specifies a method for the determination of organic isocyanates in workplace air using derivatization with di-n-butylamine (DBA) and chromatographic analysis.
This document is applicable to the determination of a wide range of organic isocyanates present in both the gas phase and the particle phase in workplace atmospheres, including monofunctional isocyanates such as isocyanic acid (ICA), methyl isocyanate (MIC), ethyl isocyanate (EIC), propyl isocyanate (PIC), butyl isocyanate (BIC) and phenyl isocyanate (PhI); monomeric diisocyanates, including 1,6-hexamethylene diisocyanate (HDI), 2,4- and 2,6-toluene diisocyanate (TDI), 4,4′-methylenediphenyl diisocyanate (MDI), 1,5-naphthyl diisocyanate (NDI), isophorone diisocyanate (IPDI) and 4,4′-dicyclohexylmethane diisocyanate (H12MDI); and multifunctional isocyanates, including oligomeric, prepolymeric and polymeric forms such as biuret-, isocyanurate- and allophanate-adducts.
The method covers air sampling using impingers, filters or combinations thereof, and analysis by liquid chromatography with mass spectrometric detection.
The useful analytical range is approximately 2,5 ng to 500 ng of isocyanate per sample. For a nominal air sample volume of 15 l, this corresponds to approximately 0,2 µg/m3 to 33 µg/m3. These values can vary depending on the isocyanate analysed.
This document does not apply to the determination of amines or aminoisocyanates. For the determination of amines and aminoisocyanates, the method specified in ISO 17734-2[11].
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This document specifies a method for the determination of the time-weighted average mass concentration of sulfuric acid and phosphoric acid in workplace air by ion chromatography. The anions are detected by conductivity.
The method is applicable to the personal sampling of airborne particles, as defined in ISO 7708, and to static (area) sampling.
The method does not apply to the determination of sulfur trioxide.
The procedure does not differentiate between the acids and their corresponding salts if both are present in the workplace air.
The procedure does not differentiate between phosphoric acid and diphosphorus pentoxide (phosphoric anhydride) if both are present in the workplace air.
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This document specifies three techniques for the determination of free Bisphenol A (BPA) in plastics of electrotechnical products.
This document describes the use of liquid chromatography–diode array detector (LC-DAD), liquid chromatography mass spectrometry (LC-MS), liquid chromatography tandem mass spectrometry (LC-MS/MS) with these test methods detailed in Annex A and Annex B.
These test methods have been evaluated for use with PC, PC/ABS, PP matrices containing free BPA between 20 mg/kg to 500 mg/kg as shown in the Pre-IIS 13 results in Annex C and IIS 13 results in Annex D [1], [2]. The use of these methods for BPA concentration ranges of plastics, other than those specified in Annex C and Annex D, has not been evaluated.
This document is a basic environment horizontal publication focusing on test methods and is primarily intended for use by committees in the preparation of publications within the area of environment in accordance with the principles laid down in IEC Guide 123. Wherever applicable, it is the responsibility of committees to make use of environment basic publications in the preparation of their environment group and product publications. Committees can apply this document directly to products when they do not develop a product publication in the area of environment.
WARNING – Persons using this document should be familiar with normal laboratory practice. This document does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user to establish appropriate safety and health practices and to ensure compliance with any national regulatory conditions.
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This document specifies a procedure for the use of quadrupole inductively coupled plasma mass spectrometry (ICP-MS), including single-quadrupole instruments and tandem ICP-MS/MS, for analysing test solutions prepared from samples of airborne particulate matter collected as specified in ISO 15202-1. Method development, performance checks and a routine analysis method are specified in this document
NOTE 1 Other types of ICP-MS (e.g. magnetic sector) are outside of the scope of this document.
Test solutions for analysis by this document are prepared as specified in ISO 15202-2.
This document is applicable to the assessment of workplace exposure to metals and metalloids for comparison with limit values (e.g. see EN 689[10] and ASTM E1370[8]).
This document is not applicable to the determination of elemental mercury, since mercury vapour is not collected using the sampling method specified in ISO 15202-1.
The procedure specified in this document is suitable for the assessment of exposure against the long-term exposure limits for most of the metals and metalloids for which occupational exposure limit values have been set, when sampling at a typical flow rate of at least 2 l min−1 for sampling times in the range 0,25 h to 8 h and for the assessment of exposure against the short-term exposure limits, where applicable.
NOTE 2 The procedure is subject to no significant spectral interferences (see Clause A.3), provided that suitable analytical isotopes are used. However, inadequate matrix-matching can adversely affect results.
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This document specifies a test method for the determination of the content of n-butyl phenyl ether (BPE, CAS: 1126-79-0, also known as butoxy-benzene) in gas oils, kerosene, diesel fuel and biodiesel blends. The method uses a two-column gas chromatograph with an FID-type of detector. The application range is 0,27 mg/l to 19,75 mg/l of BPE, with the minimum and maximum reporting levels being 0,09 mg/l and 21,89 mg/l respectively.
NOTE This corresponds to 1 % to 185 % of the average marking level of the ACCUTRACE™ Plus required by Commission Implementing Decision (EU) 2022/197 [1] of 17 January 2022 establishing a common fiscal marker for gas oils and kerosene.
The method is found to be applicable to determinations beyond this range or for specific other chemical markers that fall within the distillation temperature range of middle-distillates, but for that no precision has been determined.
WARNING — The use of this document can involve hazardous materials, operations and equipment. This document does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this document to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.
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IEC 61010-2-020:2026 is applicable to electrically powered laboratory centrifuges. It is possible that all or part of the equipment falls within the scope of one or more other Part 2 standards of IEC 61010 as well as within the scope of this document. In that case, the requirements of those other Part 2 standards will also apply. This fourth edition cancels and replaces the third edition published in 2016. This edition constitutes a technical revision.
This edition includes the following significant technical changes with respect to the previous edition:
a) alignment with changes introduced by Amendment 1:2016 of IEC 61010-1:2010.
It has the status of a product safety publication in accordance with IEC Guide 104.
This Part 2-020 is intended to be used in conjunction with the latest edition of IEC 61010-1. It was established on the basis of the third edition (2010) and its Amendment 1 (2016), hereinafter referred to as Part 1.
This Part 2-020 supplements or modifies the corresponding clauses in IEC 61010-1 so as to convert that publication into the IEC standard: Particular requirements for laboratory centrifuges.
Where a particular subclause of IEC 61010-1 is not mentioned in this Part 2-020, that subclause applies as far as is reasonable. Where this Part 2-020 states "addition", "modification" or "replacement", the relevant requirement, test specification or note in IEC 61010-1 shall be adapted accordingly.
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This document is applicable to test methods designed to be used at the place of installation of the articulated extraction arms (AEA), usually a laboratory and for various laboratory applications that require local extraction. They are used for commissioning after installation, for maintenance and for qualification purposes. For certain customer requirements additional or modified test methods can be necessary.
This document includes product functional performance referring to product standard detailed in EN 16589-1. Occupational health and safety assessments methods are not included in this document.
This document does not consider performance requirements for the extract air system associated with the AEA installation and therefore extract system performance is not part of the scope.
This document does not confirm or establish a capture zone of an AEA capture device only the functional extract capacity and mechanical functions of the AEA.
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This document specifies a method for the determination of the time-weighted average mass concentration of hydrogen chloride (HCl) gas and hydrochloric acid mist, hydrogen bromide (HBr) vapour and hydrobromic acid mist and nitric acid (HNO3) vapour and mist in workplace air by collection on an alkali-impregnated quartz fibre filter and analysis by ion chromatography.
For mist sampling, this method is applicable to the personal sampling of the inhalable fraction of airborne particles as defined in ISO 7708 and to static (area) sampling.
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This part of IEC 62321 describes the screening analysis of substances, specifically lead (Pb), mercury (Hg), cadmium (Cd), total chromium (Cr), total bromine (Br), total phosphorus (P), assuming the source of P is related to TCEP (CAS 115-96-8), Trixylyl‑phosphate (CAS 25155-23-1), total chlorine (Cl), assuming the source of Cl is related to SCCP (CAS 85535-84-8), TCEP (CAS 115-96-8) , TBTC (CAS 1461-22-9), total tin (Sn), assuming the source of Sn is related to restricted organo‑tin compounds, total antimony (Sb), assuming the source of Sb is related to Pyrochlore, and antimony lead yellow (CAS 8012-00-8) in uniform materials found in electrotechnical products, using the analytical technique of X‑ray fluorescence (XRF) spectrometry.
The same methodology can also be used for screening of substances discussed as critical raw materials in various countries (for example currently discussed in the EU: antimony (Sb), baryte, bismuth (Bi), cobalt (Co), fluorspar, gallium (Ga), germanium (Ge), hafnium (Hf), indium (In), magnesium (Mg), niobium (Nb), phosphorus (P), scandium (Sc), tantalum (Ta), tungsten (W), vanadium (V), platinum group metals, heavy rare earth elements, light rare earth elements).
NOTE From EU information on critical raw materials [1]1 raw materials are crucial to Europe's economy. They form a strong industrial base, producing a broad range of goods and applications used in everyday life and modern technologies. Reliable and unhindered access to certain raw materials is a growing concern within the EU and across the globe. To address this challenge, the European Commission has created a list of critical raw materials (CRMs) for the EU, which is subject to a regular review and update. CRMs combine raw materials of high importance to the EU economy and of high risk associated with their supply.
The method is applicable to plastics, metals and ceramic materials. The test method can be applied to raw materials, individual materials taken from products and "homogenized" mixtures of more than one material. Screening of a sample is performed using any type of XRF spectrometer, provided it has the performance characteristics specified in this test method. Not all types of XRF spectrometers are suitable for all sizes and shapes of sample. The appropriate spectrometer design will be selected with care for the task concerned.
The performance of this test method has been tested for the following substances in various media and within the concentration ranges as specified in Table 1 to Table 5. During an IIS (international interlaboratory study) the feasibility of the test method to use for the added elements was tested. The results are listed in Table 6 to Table 10.
These substances in similar media outside of the specified concentration ranges can be analysed according to this test method; however, the performance has not been established for this document.
WARNING – Persons using this International Standard should be familiar with normal laboratory practice. This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user to establish appropriate safety and health practices and to ensure compliance with any national regulatory conditions.
This document is a basic environment horizontal publication focusing on test methods and is primarily intended for use by committees in the preparation of publications within the area of environment in accordance with the principles laid down in IEC Guide 123. Wherever applicable, it is the responsibility of committees to make use of environment basic publications in the preparation of their environment group and product publications. Committees can apply this document directly to products when they do not develop a product publication in the area of environment.
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This part of IEC 62321 specifies one technique for the determination of short-chain and medium-chain chlorinated paraffins (SCCPs: C10-C13 and MCCPs: C14-C17) in plastics of electrotechnical products.
This document specifies a quantitative method for the determination of short-chain and mediumchain chlorinated paraffins in electrotechnical products by means of solvent extraction and gas chromatography-negative chemical ionization-mass spectrometry (GC-NCI-MS).
This test method has been evaluated for use with ABS (acrylonitrile butadiene styrene) and PVC (polyvinyl chloride) containing individual SCCPs ranging from 369,7 mg/kg to 8 653,9 mg/kg and MCCPs ranging from 2 141,1 mg/kg to 27 329,6 mg/kg as shown in the pre-IIS 14 results in Annex C. The use of this test method for other plastics and concentration ranges has not been specifically evaluated.
This document is a basic environment horizontal publication focusing on test methods and is primarily intended for use by committees in the preparation of publications within the area of environment in accordance with the principles laid down in IEC Guide 123. Wherever applicable, it is the responsibility of committees to make use of environment basic publications in the preparation of their environment group and product publications. Committees can apply this document directly to products when they do not develop a product publication in the area of environment.
WARNING – Persons using this International Standard should be familiar with normal laboratory practice. This International Standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user to establish appropriate safety and health practices and to ensure compliance with any national regulatory conditions.
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This document is applicable to test methods designed to be used at the place of installation of the articulated extraction arms (AEA), usually a laboratory and for various laboratory applications that require local extraction. They are used for commissioning after installation, for maintenance and for qualification purposes. For certain customer requirements additional or modified test methods can be necessary.
This document includes product functional performance referring to product standard detailed in EN 16589-1. Occupational health and safety assessments methods are not included in this document.
This document does not consider performance requirements for the extract air system associated with the AEA installation and therefore extract system performance is not part of the scope.
This document does not confirm or establish a capture zone of an AEA capture device only the functional extract capacity and mechanical functions of the AEA.
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This document defines terms related with the production and use of reference materials including certified reference materials.
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This document specifies a method for the determination of selected polybrominated diphenylethers (PBDE) (see Figure 1 and Table 1) in sediment, suspended particulate matter and biota using gas chromatography coupled with tandem mass spectrometry (GC-MS/MS) or with high resolution mass spectrometry (GC-HRMS) in the electron impact (EI), negative ion chemical ionization (NCI) or atmospheric pressure ionization (APCI) mode.
The method is applicable to sediment and suspended particulate matter samples with limits of quantification of 0,2 µg/kg dry mass (dm) for brominated diphenylether (BDE) BDE-28 to BDE-183, of 2 µg/kg dry mass (dm) for BDE‑209.
The method is applicable as well with lower limits of quantification (LOQ), if specific clean-up methods, described in Clause 10, Table 3, method 1 and method 2 in combination with measurement methods GC-MS/MS or GC-HRMS after electron impact ionization (El) or negative ion chemical ionization (NCI) for BDE-209 are used. Depending on the analytical capability of the instrument, limits of quantification down to 0,003 µg/kg dm for BDE-28 to BDE-154 and 0,02 µg/kg dm for BDE-183 and 1 µg/kg dm for BDE-209 and lower are possible.
The method is applicable to biota samples with limits of quantification down to 0,000 2 µg/kg fresh mass (fm) (BDE-28 to BDE-154) and 0,03 μg/kg fresh mass (fm) (BDE-183), if specific clean-up methods, described in Table 4 in combination with measurement methods GC-MS/MS or GC-HRMS after electron impact ionization (El) are used.
Performance data are listed in Annex E.
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This document specifies a gas chromatographic method for ethanol, in which higher alcohols (propan-1-ol, butan-1-ol, butan-2-ol, 2-methylpropan-1-ol (iso-butanol), 2-methylbutan-1-ol, and 3-methylbutan-1-ol) from (0,1 up to 2,5) mass percentage, methanol from (0,1 up to 3) mass percentage and other impurities, in the range from (0,1 up to 2) mass percentage are determined.
NOTE 1 The European ethanol blending component specification [1] sets a limit for the combined result of ethanol + higher alcohols, not the ethanol content itself.
The method is developed for non-denatured ethanol samples. With sufficient attention to correct separation of the higher alcohols and other components, determination of hydrocarbons in ethanol that contains denaturants as per EN 15376 [1] is possible.
NOTE 2 For the purposes of this document, the term “% (m/m)” is used to represent the mass percentage or mass fraction (ω).
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This document specifies a method for determining the total content (solvent extractable) of melamine in chemicals for the leather tanning industry.
This method requires the use of liquid chromatography (LC) with a triple quadrupole mass spectrometer (MS/MS), an ultraviolet (UV) detector, or diode array detector (DAD) to identify and quantify the melamine.
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This document specifies a method for determining the total content (solvent extractable) of melamine in chemicals for the leather tanning industry.
This method requires the use of liquid chromatography (LC) with a triple quadrupole mass spectrometer (MS/MS), an ultraviolet (UV) detector, or diode array detector (DAD) to identify and quantify the melamine.
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This document specifies a test method for determination of aldehydes in propylene oxide by liquid chromatography. This document is applicable to the determination of aldehydes in propylene oxide for industrial use, including formaldehyde, acetaldehyde, propionaldehyde and acrolein. The concentration for each aldehyde ranges from 0,5 mg/kg to 100 mg/kg.
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This document specifies a test method for the determination of propylene oxide and trace impurities in propylene oxide for industrial use by gas chromatography. This document is suitable for the determination of propylene oxide which is produced by ethylbenzene co-oxidation (PO/SM), isobutane co-oxidation (PO/TBA), cumene co-oxidation (CHPPO), hydrogen peroxide oxidation (HPPO) and chlorohydrin. This document is applicable for determination of propylene oxide with a purity ≥ 99,70 % and impurity content ≥ 0,000 3 %.
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This document specifies the determination of Cr(VI) in solid waste material and soil by alkaline digestion and ion chromatography with spectrophotometric detection. This method can be used to determine Cr(VI)-mass fractions in solids higher than 0,1 mg/kg.
NOTE In case of reducing or oxidising waste matrix no valid Cr(VI) content can be reported.
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This document specifies a method for the determination of the following elements in aqua regia, nitric acid or mixture of hydrochloric (HCl), nitric (HNO3) and tetrafluoroboric (HBF4)/hydrofluoric (HF) acid digests of soil, treated biowaste, waste, sludge and sediment:
aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium (Cd), calcium (Ca), cerium (Ce), caesium (Cs), chromium (Cr), cobalt (Co), copper (Cu), dysprosium (Dy), erbium (Er), europium (Eu), gadolinium (Gd), gallium (Ga), germanium (Ge), gold (Au), hafnium (Hf), holmium (Ho), indium (In), iridium (Ir), iron (Fe), lanthanum (La), lead (Pb), lithium (Li), lutetium (Lu), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), neodymium (Nd), nickel (Ni), palladium (Pd), phosphorus (P), platinum (Pt), potassium (K), praseodymium (Pr), rhenium (Re), rhodium (Rh), rubidium (Rb), ruthenium (Ru), samarium (Sm), scandium (Sc), selenium (Se), silicon (Si), silver (Ag), sodium (Na), strontium (Sr), sulfur (S), tellurium (Te), terbium (Tb), thallium (Tl), thorium (Th), thulium (Tm), tin (Sn), titanium (Ti), tungsten (W), uranium (U), vanadium (V), ytterbium (Yb), yttrium (Y), zinc (Zn), and zirconium (Zr).
NOTE 1 Details on validation are given in Annex A.
This method is also applicable for the determination of major, minor and trace elements in aqua regia and nitric acid digests and in eluates of construction products (EN 17200[7]).
NOTE 2 Construction products include e.g. mineral-based products, bituminous products, metals, wood-based products, plastics and rubbers, sealants and adhesives, paints and coatings.
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This document gives an overview of a variety of physical and analytical methods by which bacteria, biofilms, and the interaction of those with antimicrobial compounds can be analysed. For each technique a general overview is given and its current state of the art. The strengths and limitations of each technique to measure microbial samples are given alongside suggestions for future developments. This document is intended as a guide and a starting point to more specific activities of ISO/TC 201, Surface chemical analysis, in the future, which end in standardized procedures for measurements.
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This document is a product specification, giving performance requirements for emergency safety body showers connected to the water supply. It is applicable to plumbed-in body showers only, located in laboratory facilities.
Requirements are given in respect of the performance, installation, adjustment and marking of the showers as well as installation, operation and maintenance instructions to be given by the manufacturer.
NOTE Attention is drawn to national regulations which might apply in respect of the installation and use of emergency safety showers.
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This document is a product specification, giving performance requirements for emergency safety eyewash units connected to the water supply. It is applicable to plumbed-in eyewash units only.
Requirements are given in respect of the performance, installation, adjustment and marking of the eyewash units, as well as installation, operation and maintenance instructions to be given by the manufacturer.
NOTE Attention is drawn to national regulations which can apply in respect of the installation and use of eyewash units.
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This document is a product specification, giving performance requirements for emergency safety body showers connected to the water supply. It is applicable to plumbed-in body showers only, located in laboratory facilities.
Requirements are given in respect of the performance, installation, adjustment and marking of the showers as well as installation, operation and maintenance instructions to be given by the manufacturer.
NOTE Attention is drawn to national regulations which might apply in respect of the installation and use of emergency safety showers.
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This document is a product specification, giving performance requirements for emergency safety eyewash units connected to the water supply. It is applicable to plumbed-in eyewash units only.
Requirements are given in respect of the performance, installation, adjustment and marking of the eyewash units, as well as installation, operation and maintenance instructions to be given by the manufacturer.
NOTE Attention is drawn to national regulations which can apply in respect of the installation and use of eyewash units.
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This document defines the core terms and definitions in the field of laboratory design.
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This document specifies methods for:
— determining the composition of a calibration gas mixture by comparison with appropriate reference gas mixtures;
— calculating the uncertainty of the composition of a calibration gas mixture in relation to the known uncertainty of the composition of the reference gas mixtures with which it was compared;
— checking the composition attributed to a calibration gas mixture by comparison with appropriate reference gas mixtures;
— consistency testing and outlier search in suites of calibration gas mixtures of closely related composition.
NOTE 1 In principle, the method described in this document is also applicable to the analysis of (largely) unknown samples instead of prospective calibration gas mixtures (i.e. gas mixtures which are intended for use as calibration gas mixtures). Such applications, however, need appropriate care and consideration of additional uncertainty components, for example, concerning the effect of matrix differences between the reference gases used for calibration and the analysed sample.
NOTE 2 Comparison methods based on one- and two-point calibration are described in ISO 12963.
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This document specifies the methods for the chemical analysis of cement.
This document describes the reference methods and, in certain cases, an alternative method which can be considered to be equivalent. In the case of a dispute, only the reference methods are used.
An alternative performance-based method using X-ray fluorescence (XRF) is described for SiO2, Al2O3, Fe2O3, CaO, MgO, SO3, K2O, Na2O, TiO2, P2O5, Mn2O3, SrO, Cl and Br. This method is based on beads of fused sample and analytical validation using certified reference materials, together with performance criteria. A method based on pressed pellets of un-fused sample can be considered as equivalent, providing that the analytical performance satisfies the same criteria.
An alternative performance-based method using inductively coupled plasma optical emission spectroscopy (ICP-OES) is described for SO3.
When correctly calibrated according to the specified procedures and reference materials, XRF and ICP-OES provides methods equivalent to the reference methods but has not been validated for use yet as a reference procedure for conformity and dispute purposes. They can be applied to other relevant elements when adequate calibrations have been established.
Any other methods can be used provided they are calibrated, either against the reference methods or against internationally accepted reference materials, in order to demonstrate their equivalence.
This document describes methods which apply principally to cements, but which can also be applied to their constituent materials. They can also be applied to other materials, the standards for which call up these methods. Standard specifications state which methods are to be used.
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This document specifies a method using gas chromatography with mass selective detector (GC-MS) for detection and quantification of extractable N,N-dimethylformamide (DMF), N,N-dimethylacetamide (DMAC), N-methyl-2-pyrrolidone (NMP) and N-ethyl-2-pyrrolidone (NEP) in filaments and coatings of textile products.
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This document gives guidance on sample preparation, and on qualitative and quantitative determination of elements in particulate matter collected on filtering membranes (PM filter) by energy dispersive X-ray Fluorescence (EDXRF) in different geometrical configurations. This document does not apply to PM filter sampling. This document only applies to the analysis of X-ray emission from filters that are probed using an X-ray beam as the exciting source. X-ray emissions generated by electron microscope are excluded[1]. This document is applicable under a range of contexts including, but not limited to, those highlighted in the introduction. The described method is generally applicable for the determination of elements with atomic number higher than 11 (Na) and having a deposited mass on the filter greater than 10 ng. The elements that can be identified and the detection limits depend on the specific instrumental configuration employed. Various types of filtering membranes (filter) materials can be used, such as glass fibre, quartz fibre, cellulose, nylon, polycarbonate (PC) and polytetrafluoroethylene (PTFE). The entire filter, or portions of various sizes thereof, can be submitted for analysis. NOTE Reference free analysis, based on fundamental parameters is excluded, as the nature of the PM filter samples means that the parameters are not sufficiently well defined.
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This document is applicable to biology, chemistry and physics laboratories where research, preparative, analytical, process activities take place and which can involve work with hazardous substances, including higher education (college and university teaching and post-graduate research).
This document does not cover the requirements of schools, i.e. precollege/pre-university (refer to EN 13150), or highly specialist laboratories which need very specific, bespoke solutions to enable them to function.
This document specifies requirements for installation and design of laboratory benches, associated storage units, and for the provision and connection of services integral or delivered to the laboratory benches. This document gives guidelines for all parties involved in the planning, design, manufacture, installation, testing of a new laboratory or in the refurbishment of an existing laboratory.
For safety storage cabinets for flammable liquids EN 14470-1 and for pressurized gas cylinders EN 14470-2 applies.
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This document is applicable to recirculatory filtration fume cabinets (RFFC).
Recirculatory filtration fume cabinets are devices intended to protect their users by means of:
— the ability to contain hazardous concentrations or quantities of airborne contaminants;
— the ability to remove hazardous concentrations or quantities of airborne contaminants from air exhausted from inside the fume cabinet by means of filtration before the air is recirculated to the room in which the fume cabinet is located.
This document specifies design and manufacturing requirements together with type and on-site testing procedures.
This document does not specify requirements for the use of a mixture of chemicals but provides guidance on how to proceed.
NOTE For special applications and usage such as Carcinogenic, Mutagenic, Reprotoxic Substances (CMR) substances, local regulation can apply. These local regulations can result on restriction of usage.
This document is not intended to address fume cupboards, or devices used as animal accommodation. For fume cupboards, the EN 14175 series applies. For microbiological safety cabinets, EN 12469 applies.
- Standard31 pagesEnglish languagee-Library read for1 day
The document provides the physical principles and specifies instrumental requirements for total reflection X‑ray fluorescence analysis (TXRF) spectrometers. This document specifies general procedures for calibration, method development and verification of TXRF measurements and quality control. The document describes measurements with TXRF conditions having a fixed glancing angle below the critical angle of total reflection and considerably enhanced excitation radiation intensity. Although certain definitions of grazing incidence geometry are shown for clarification, this document is not applicable to measurement setups working under such conditions.
- Standard22 pagesEnglish languagesale 15% off
This document is applicable to biology, chemistry and physics laboratories where research, preparative, analytical, process activities take place and which can involve work with hazardous substances, including higher education (college and university teaching and post-graduate research).
This document does not cover the requirements of schools, i.e. precollege/pre-university (refer to EN 13150), or highly specialist laboratories which need very specific, bespoke solutions to enable them to function.
This document specifies requirements for installation and design of laboratory benches, associated storage units, and for the provision and connection of services integral or delivered to the laboratory benches. This document gives guidelines for all parties involved in the planning, design, manufacture, installation, testing of a new laboratory or in the refurbishment of an existing laboratory.
For safety storage cabinets for flammable liquids EN 14470-1 and for pressurized gas cylinders EN 14470-2 applies.
- Standard39 pagesEnglish languagee-Library read for1 day
This document is applicable to recirculatory filtration fume cabinets (RFFC).
Recirculatory filtration fume cabinets are devices intended to protect their users by means of:
— the ability to contain hazardous concentrations or quantities of airborne contaminants;
— the ability to remove hazardous concentrations or quantities of airborne contaminants from air exhausted from inside the fume cabinet by means of filtration before the air is recirculated to the room in which the fume cabinet is located.
This document specifies design and manufacturing requirements together with type and on-site testing procedures.
This document does not specify requirements for the use of a mixture of chemicals but provides guidance on how to proceed.
NOTE For special applications and usage such as Carcinogenic, Mutagenic, Reprotoxic Substances (CMR) substances, local regulation can apply. These local regulations can result on restriction of usage.
This document is not intended to address fume cupboards, or devices used as animal accommodation. For fume cupboards, the EN 14175 series applies. For microbiological safety cabinets, EN 12469 applies.
- Standard31 pagesEnglish languagee-Library read for1 day
This document specifies a method to optimize the mass calibration accuracy in time-of-flight secondary ion mass spectrometry (SIMS) instruments used for general analytical purposes. This document is only applicable to time-of-flight instruments but is not restricted to any particular instrument design. This document gives guidance for some of the instrumental parameters that can be optimized using this procedure and the types of generic peaks suitable to calibrate the mass scale for optimum mass accuracy.
- Standard13 pagesEnglish languagesale 15% off
This document specifies a method using energy-dispersive X-ray fluorescence spectrometry for the determination of the sulfur content of petroleum products, such as naphthas, unleaded motor gasolines, middle distillates, residual fuel oils, base lubricating oils and components. The method is applicable to products with sulfur content in the range of a mass fraction of 0,03 % to a mass fraction of 5,00 %.
This test method can be used for biofuel or biofuel blends.
- Standard17 pagesEnglish languagee-Library read for1 day
This document specifies a wavelength-dispersive X-ray fluorescence (WDXRF) test method for the determination of the sulfur content in ethanol (E85) automotive fuel [3], containing ethanol between 50 % (V/V) and 85 % (V/V), from 5 mg/kg to 20 mg/kg, using instruments with either monochromatic or polychromatic excitation.
NOTE 1 Sulfur contents higher than 20 mg/kg can be determined after sample dilution with an appropriate solvent. However, the precision was not established for diluted samples.
NOTE 2 For the purposes of this document, the terms "% (m/m)" and "% (V/V)" are used to represent the mass fraction (µ) and the volume fraction (φ) of a material respectively.
WARNING - The use of this document can involve hazardous materials, operations and equipment. This document does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this document to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Standard14 pagesEnglish languagee-Library read for1 day
This document defines the following quantities commonly used to express the composition of gas mixtures:
— amount fraction and concentration;
— mass fraction and concentration;
— volume fraction and concentration.
For these quantities of composition, this document specifies methods for:
— conversion between different quantities;
— conversion between different state conditions.
Conversion between different quantities means calculating the value of the content of a specified component in terms of one of the quantities listed above from the value of the same content, at the same pressure and temperature of the gas mixture, given in terms of another of these quantities. Conversion between different state conditions means calculating the value of the content of a specified component, in terms of one of the quantities listed above, under one set of state conditions from the value of the same quantity under another set of state conditions, i.e., pressure and temperature, of the gas mixture. Gas mixture composition can be converted simultaneously between different quantities of composition and different state conditions by combination of the two types of conversion.
This document is applicable only to homogeneous and stable gas mixtures. Therefore, any state conditions (pressure and temperature) considered need to be well outside the condensation region of the gas mixture. In addition, volume concentrations can only be used if the component under consideration is completely gaseous, and for the use of volume fractions, all components need to be completely gaseous. Further restrictions of state conditions apply for approximations of compression factors using virial coefficients (see Annex A).
- Standard63 pagesEnglish languagee-Library read for1 day
This document specifies methods for quantitative determination of seven selected polychlorinated biphenyls (PCB28, PCB52, PCB101, PCB118, PCB138, PCB153 and PCB180) in soil, sludge, sediment, treated biowaste, and waste using GC-MS and GC-ECD (see Table 2).
The limit of detection depends on the determinants, the equipment used, the quality of chemicals used for the extraction of the sample and the clean-up of the extract.
Under the conditions specified in this document, lower limit of application from 1 μg/kg (expressed as dry matter) for soils, sludge and biowaste to 10 μg/kg (expressed as dry matter) for solid waste can be achieved. For some specific samples the limit of 10 μg/kg cannot be reached.
Sludge, waste and treated biowaste may differ in properties, as well as in the expected contamination levels of PCB and presence of interfering substances. These differences make it impossible to describe one general procedure. This document contains decision tables based on the properties of the sample and the extraction and clean-up procedure to be used.
NOTE The analysis of PCB in insulating liquids, petroleum products, used oils and aqueous samples is referred to in EN 61619, EN 12766-1 and ISO 6468 respectively.
The method can be applied to the analysis of other PCB congeners not specified in the scope, provided suitability is proven by proper in-house validation experiments.
- Standard50 pagesEnglish languagee-Library read for1 day
This document specifies a glow discharge optical emission spectrometric (GD-OES) method for the determination of the thickness, mass per unit area and chemical composition of surface layer films. The applicability of this document is limited to description of general procedures for quantification of the chemical composition and thickness in GD-OES compositional depth profiling. This document is not directly applicable for quantification of individual materials having various thicknesses and elements to be determined.
- Standard34 pagesEnglish languagesale 15% off
This document specifies methods for:
— determining the composition of a calibration gas mixture by comparison with appropriate reference gas mixtures;
— calculating the uncertainty of the composition of a calibration gas mixture in relation to the known uncertainty of the composition of the reference gas mixtures with which it was compared;
— checking the composition attributed to a calibration gas mixture by comparison with appropriate reference gas mixtures;
— consistency testing and outlier search in suites of calibration gas mixtures of closely related composition.
NOTE 1 In principle, the method described in this document is also applicable to the analysis of (largely) unknown samples instead of prospective calibration gas mixtures (i.e. gas mixtures which are intended for use as calibration gas mixtures). Such applications, however, need appropriate care and consideration of additional uncertainty components, for example, concerning the effect of matrix differences between the reference gases used for calibration and the analysed sample.
NOTE 2 Comparison methods based on one- and two-point calibration are described in ISO 12963.
- Standard50 pagesEnglish languagee-Library read for1 day
This document specifies methods for: — determining the composition of a calibration gas mixture by comparison with appropriate reference gas mixtures; — calculating the uncertainty of the composition of a calibration gas mixture in relation to the known uncertainty of the composition of the reference gas mixtures with which it was compared; — checking the composition attributed to a calibration gas mixture by comparison with appropriate reference gas mixtures; — consistency testing and outlier search in suites of calibration gas mixtures of closely related composition. NOTE 1 In principle, the method described in this document is also applicable to the analysis of (largely) unknown samples instead of prospective calibration gas mixtures (i.e. gas mixtures which are intended for use as calibration gas mixtures). Such applications, however, need appropriate care and consideration of additional uncertainty components, for example, concerning the effect of matrix differences between the reference gases used for calibration and the analysed sample. NOTE 2 Comparison methods based on one- and two-point calibration are described in ISO 12963.
- Standard41 pagesEnglish languagesale 15% off
- Standard41 pagesFrench languagesale 15% off
This document provides symbols and defines standard datasheets for some of the most often used microfluidic pumps, such as the peristaltic pump, pressure pump, syringe pump and diaphragm/membrane pump.
- Technical specification14 pagesEnglish languagesale 15% off
This document specifies a chemical method for technicians working with total reflection X-ray fluorescence (TXRF) instrumentation to perform measurements of water samples, according to good practices, with a defined degree of accuracy and precision. Target users are identified among laboratories performing routine analysis of large numbers of samples, which also conform with ISO/IEC 17025. This document specifies a method to determine the content of elements dissolved in water (e.g. drinking water, surface water and ground water). This document is also applicable for determining elements in waste waters and eluates, taking into account the specific and additionally occurring interferences. This document does not specify sampling, dilution and pre-concentration methods. Elements determined using the method specified in this document can depend on the X-ray source of the instrument. This document does not specify health, safety or commercial aspects. The determinable concentrations depend on the matrix and the interferences encountered. In drinking water and relatively unpolluted waters, the limit of quantification lies between 0,001 mg/l and 0,01 mg/l for most of the elements. The range of concentrations typically lies between 0,001 mg/l and 10 mg/l, depending on the element and predefined requirements. Annex A reports an example of uncertainty calculation. Annex B provides an example report on validation of the method for TXRF analysis of water performed with instrumentation that has Mo as the X-ray source and uses Ga as the internal calibration standard. Limits of quantification of most elements are affected by blank contamination and depend predominantly on the laboratory air-handling facilities available, on the purity of reagents and the cleanliness of labware.
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This document defines the most commonly used terms for transmission electron microscopy (TEM) specimen preparation using focused ion beam (FIB).
- Standard14 pagesEnglish languagesale 15% off
This document defines the following quantities commonly used to express the composition of gas mixtures:
— amount fraction and concentration;
— mass fraction and concentration;
— volume fraction and concentration.
For these quantities of composition, this document specifies methods for:
— conversion between different quantities;
— conversion between different state conditions.
Conversion between different quantities means calculating the value of the content of a specified component in terms of one of the quantities listed above from the value of the same content, at the same pressure and temperature of the gas mixture, given in terms of another of these quantities. Conversion between different state conditions means calculating the value of the content of a specified component, in terms of one of the quantities listed above, under one set of state conditions from the value of the same quantity under another set of state conditions, i.e., pressure and temperature, of the gas mixture. Gas mixture composition can be converted simultaneously between different quantities of composition and different state conditions by combination of the two types of conversion.
This document is applicable only to homogeneous and stable gas mixtures. Therefore, any state conditions (pressure and temperature) considered need to be well outside the condensation region of the gas mixture. In addition, volume concentrations can only be used if the component under consideration is completely gaseous, and for the use of volume fractions, all components need to be completely gaseous. Further restrictions of state conditions apply for approximations of compression factors using virial coefficients (see Annex A).
- Standard63 pagesEnglish languagee-Library read for1 day