ASTM D8125-18
(Specification)Standard Specification for Re-Refined Engine Oil Bottoms (REOB)/Vacuum Tower Asphalt Extender (VTAE)
Standard Specification for Re-Refined Engine Oil Bottoms (REOB)/Vacuum Tower Asphalt Extender (VTAE)
ABSTRACT
This specification establishes the material, manufacturing, and physical requirements for re-refined engine oil bottoms, also known as vacuum tower asphalt extender, that may be used in formulating asphalt for pavement construction and roofing. ”Re-refined engine oil bottoms” (REOB) is the commonly used term used by many state highway agencies and FHWA, while ”vacuum tower asphalt extender” (VTAE) is preferred by manufacturers. REOB/VTAE may be obtained by processing used engine oil using atmospheric distillation followed by vacuum distillation to produce a vacuum residuum meeting the requirements outlined in this specification. The REOB/VTAE shall be homogenous, free from water, and not foam when heated to 232°C (450°F).
This specification also covers the methods of sampling and testing for REOB/VTAE.
SCOPE
1.1 This specification covers re-refined engine oil bottoms, also known as vacuum tower asphalt extender, that may be used in formulating asphalt for pavement construction and roofing. This specification has been developed specifically for these two categories of product and is not intended for other uses. Table 1 is to be used for pavement construction and Table 2 for roofing. “Re-refined engine oil bottoms” (REOB) is the prevailing name used by many state highway agencies and FHWA, while “vacuum tower asphalt extender” (VTAE) is the preferred name used by the manufacturers of the product. Since each name provides an important descriptor of production elements (“re-refined” and “vacuum tower”) for the specific product this specification addresses, this specification uses the term “REOB/VTAE.”
1.2 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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Designation: D8125 − 18
Standard Specification for
Re-Refined Engine Oil Bottoms (REOB)/Vacuum Tower
1
Asphalt Extender (VTAE)
This standard is issued under the fixed designation D8125; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 2. Referenced Documents
2
1.1 This specification covers re-refined engine oil bottoms, 2.1 ASTM Standards:
also known as vacuum tower asphalt extender, that may be D92 Test Method for Flash and Fire Points by Cleveland
used in formulating asphalt for pavement construction and Open Cup Tester
roofing. This specification has been developed specifically for D93 Test Methods for Flash Point by Pensky-Martens
these two categories of product and is not intended for other Closed Cup Tester
uses. Table 1 is to be used for pavement construction and Table D95 Test Method for Water in Petroleum Products and
2 for roofing. “Re-refined engine oil bottoms” (REOB) is the Bituminous Materials by Distillation
prevailing name used by many state highway agencies and D140/D140M Practice for Sampling Asphalt Materials
FHWA, while “vacuum tower asphalt extender” (VTAE) is the D2042 Test Method for Solubility of Asphalt Materials in
preferred name used by the manufacturers of the product. Since Trichloroethylene
each name provides an important descriptor of production D2872 Test Method for Effect of Heat and Air on a Moving
elements (“re-refined” and “vacuum tower”) for the specific Film of Asphalt (Rolling Thin-Film Oven Test)
product this specification addresses, this specification uses the D4402/D4402M Test Method for Viscosity Determination of
term “REOB/VTAE.” Asphalt at Elevated Temperatures Using a Rotational
Viscometer
1.2 Units—The values stated in either SI units or inch-
D7553 Test Method for Solubility of Asphalt Materials in
pound units are to be regarded separately as standard. The
N-Propyl Bromide
values stated in each system may not be exact equivalents;
D8078 Test Method for Ash Content of Asphalt and Emul-
therefore, each system shall be used independently of the other.
sified Asphalt Residues
Combining values from the two systems may result in noncon-
E1131 Test Method for Compositional Analysis by Thermo-
formance with the standard.
gravimetry
1.3 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
3. Materials and Manufacture
responsibility of the user of this standard to establish appro-
3.1 REOB/VTAE shall be the product of processing used
priate safety, health, and environmental practices and deter-
engine oil using atmospheric distillation followed by vacuum
mine the applicability of regulatory limitations prior to use.
distillation to produce a vacuum residuum meeting the speci-
1.4 This international standard was developed in accor-
fications outlined in Table 1 or Table 2.
dance with internationally recognized principles on standard-
ization established in the Decision on Principles for the
4. Physical Requirements
Development of International Standards, Guides and Recom-
4.1 The REOB/VTAE shall be homogenous, free from
mendations issued by the World Trade Organization Technical
water, and not foam when heated to 232 °C (450 °F).
Barriers to Trade (TBT) Committee.
4.2 The REOB/VTAE shall conform to the requirements
given in Table 1 or Table 2 based on the intended end use.
1
This specification is under the jurisdiction of ASTM Committee D04 on Road
and Paving Materials and is the direct responsibility of Subcommittee D04.40 on
2
Asphalt Specifications. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved July 1, 2018. Published July 2018. Originally approved contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
in 2017. Last previous edition approved in 2017 as D8125 – 17. DOI: 10.1520/ Standards volume information, refer to the standard’s Document Summary page on
D8125-18. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D8125 − 18
TABLE 1 Requirements for REOB/VTAE Used in Pavement TABLE 2 Requirements for REOB/VTAE Used in Roofing
Construction
Test
Flash Point, Cleveland Open Cup, min, °C (°F) >274 (525)
Test
Flash Point, Pensky Martin Closed Cup, min, °C (°F) >232 (450)
Flash Point, Cleveland Open Cup, min, °C (°F) >232 (450)
Mass Change, RTFOT, % w/w max 1.0
Mass Change, RTFOT, % w/w max 1.0
A
A
Solubility, min, % 98.0 Solubility, min, % 98.0
B
B
Viscosity, 60 °C (140 °F), cP 200 – 5
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D8125 − 17 D8125 − 18
Standard Specification for
Re-Refined Engine Oil Bottoms (REOB)/Vacuum Tower
1
Asphalt Extender (VTAE)
This standard is issued under the fixed designation D8125; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This specification covers re-refined engine oil bottoms, also known as vacuum tower asphalt extender, that may be used in
formulating asphalt for pavement construction and roofing. This specification has been developed specifically for these two
categories of product and is not intended for other uses. Table 1 is to be used for pavement construction and Table 2 for roofing.
“Re-refined engine oil bottoms” (REOB) is the prevailing name used by many state highway agencies and FHWA, while “vacuum
tower asphalt extender” (VTAE) is the preferred name used by the manufacturers of the product. Since each name provides an
important descriptor of production elements (“re-refined” and “vacuum tower”) for the specific product this specification addresses,
this specification uses the term “REOB/VTAE.”
1.2 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated
in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values
from the two systems may result in nonconformance with the standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of
regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
D92 Test Method for Flash and Fire Points by Cleveland Open Cup Tester
D93 Test Methods for Flash Point by Pensky-Martens Closed Cup Tester
D95 Test Method for Water in Petroleum Products and Bituminous Materials by Distillation
D140/D140M Practice for Sampling Asphalt Materials
D2042 Test Method for Solubility of Asphalt Materials in Trichloroethylene
D2872 Test Method for Effect of Heat and Air on a Moving Film of Asphalt (Rolling Thin-Film Oven Test)
D4402/D4402M Test Method for Viscosity Determination of Asphalt at Elevated Temperatures Using a Rotational Viscometer
D7553 Test Method for Solubility of Asphalt Materials in N-Propyl Bromide
D8078 Test Method for Ash Content of Asphalt and Emulsified Asphalt Residues
E1131 Test Method for Compositional Analysis by Thermogravimetry
3. Materials and Manufacture
3.1 REOB/VTAE shall be the product of processing used engine oil using atmospheric distillation followed by vacuum
distillation to produce a vacuum residuum meeting the specifications outlined in Table 1 or Table 2.
1
This specification is under the jurisdiction of ASTM Committee D04 on Road and Paving Materials and is the direct responsibility of Subcommittee D04.40 on Asphalt
Specifications.
Current edition approved Oct. 1, 2017July 1, 2018. Published October 2017July 2018. Originally approved in 2017. Last previous edition approved in 2017 as D8125 – 17.
DOI: 10.1520/D8125-17.10.1520/D8125-18.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D8125 − 18
TABLE 1 Requirements for REOB/VTAE Used in Pavement
Construction
Test
Flash Point, Cleveland Open Cup, min, °C (°F) >232 (450)
Mass Change, RTFOT, % w/w max 1.0
A
Solubility, min, % 98.0
B
Viscosity, 60 °C (140 °F), cP 200 – 5000
CD
Ash Content, max, % 6.0
CD
Ash Content, max, % 7.0
A
The 98 % solubility requirement applies to the REOB/VTAE component only. This
requirement may be waived by the purchaser i
...








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