D04.44 - Rheological Tests

SIGNIFICANCE AND USE
5.1 The kinematic viscosity characterizes flow behavior. The method is used to determine the consistency of liquid asphalt as one element in establishing the uniformity of shipments or sources of supply. The specifications are usually at temperatures of 60 and 135 °C.
Note 3: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method covers procedures for the determination of kinematic viscosity of liquid asphalts, road oils, and distillation residues of liquid asphalts all at 60 °C [140 °F] and of liquid asphalt binders at 135 °C [275 °F] (see table notes, 11.1) in the range from 6 to 100 000 mm2/s [cSt].  
1.2 Results of this test method can be used to calculate viscosity when the density of the test material at the test temperature is known or can be determined. See Annex A1 for the method of calculation.  
Note 1: This test method is suitable for use at other temperatures and at lower kinematic viscosities, but the precision is based on determinations on liquid asphalts and road oils at 60 °C [140 °F] and on asphalt binders at 135 °C [275 °F] only in the viscosity range from 30 to 6000 mm2/s [cSt].
Note 2: Modified asphalt binders or asphalt binders that have been conditioned or recovered are typically non-Newtonian under the conditions of this test. The viscosity determined from this method is under the assumption that asphalt binders behave as Newtonian fluids under the conditions of this test. When the flow is non-Newtonian in a capillary tube, the shear rate determined by this method may be invalid. The presence of non-Newtonian behavior for the test conditions can be verified by measuring the viscosity with viscometers having different-sized capillary tubes. The defined precision limits in 11.1 may not be applicable to non-Newtonian asphalt binders.  
1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency (EPA) and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Material Safety Data Sheet (MSDS) or Safety Data Sheet (SDS) for details and the EPA’s website—http://www.epa.gov/mercury/faq.htm—for additional information. Users should be aware that selling mercury, mercury-containing products, or both, in your state may be prohibited by state law.  
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.5 The text of this standard references notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior ...

SIGNIFICANCE AND USE
4.1 This test method is useful in confirming that an asphalt cement has been modified with a material that provides a significant elastomeric component. Elastomer-modified asphalts can be characterized by their ability to be stretched to a large elongation while at the same time resisting further stretching. Toughness and tenacity are two parameters for measuring this ability.
Note 1: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method describes the procedure for measuring the toughness and tenacity of asphalt materials. Typically, the test method has been used to characterize elastomer-modified asphalts, although values for toughness and tenacity may be obtained for any type of polymer-modified or non-modified asphalt.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.2.1 Exception—Sample mass is given only in SI units. Sample mass as given in SI units should be regarded as standard. No other units of sample mass are included in this standard.  
1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable Material Safety Data Sheet (MSDS) for details and EPA’s website—http://www.epa.gov/mercury/index.htm—for additional information. Users should be aware that selling mercury and/or mercury-containing products in your state may be prohibited by state law.  
1.4 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 The complex shear modulus is an indicator of the stiffness or resistance of asphalt binder to deformation under load. The phase angle is a measure of the relative portion of the response to an applied load that is elastic (recoverable) or viscous (nonrecoverable).  
5.2 The test procedure is applicable to measurements in the linear region where the measured modulus and phase angle are independent of the amplitude of the strain.  
5.3 The complex modulus and the phase angle are used to calculate performance-related criteria in accordance with Specification D6373 or D8239.
Note 1: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method covers the determination of the complex shear modulus and phase angle of asphalt binders when tested in dynamic (oscillatory) shear using parallel plate geometry.  
1.2 This test method is intended for determining the linear viscoelastic properties of asphalt binders as required for specification testing and is not intended as a comprehensive procedure for the full characterization of the viscoelastic properties of asphalt binder.  
1.3 This standard is appropriate for unaged asphalt binder, conditioned asphalt binder, and asphalt binder recovered from either asphalt mixtures or asphalt emulsions. To keep the language in this standard precise, the term “asphalt binder” is used to refer to the material being tested.  
1.4 This procedure is limited to asphalt binders that contain particles with largest dimension less than 250 μm.  
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.6 Warning—Mercury has been designated by the United States Environmental Protection Agency (EPA) and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for details and EPA’s website— www.epa.gov/mercury/faq.htm—for additional information. Users should be aware that selling mercury, mercury-containing products, or both, into your state may be prohibited by state law.  
1.7 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 This test is primarily used for field production control of asphalt-rubber (A-R) and other high-viscosity binders; however, the test can also be used in a laboratory setting.  
3.2 A handheld rotational viscometer is used to measure the apparent viscosity of a completed blend of A-R or high-viscosity binder. A rotor (spindle), turning at constant speed, is inserted in the liquid binder to be measured. The resistance to movement of the spindle (torque) caused by the viscosity of the surrounding liquid is measured using a special mechanism to obtain direct readings in Pa·s or cP.
Note 1: Spindle is generally made of stainless steel, although another metal such as brass could be used.  
3.3 The measured apparent viscosity is used to control the production of the A-R or other high-viscosity binder, to assess the uniformity of the binder produced, or for other related purposes.  
3.4 As the spindle turns in the A-R or other high-viscosity binder, it has a tendency to “drill” into the sample (that is, for A-R, the spindle spins the rubber particles out of the measurement area). Consequently, the apparent viscosity drops to reflect only the liquid phase of the high-viscosity binder. Therefore, the peak viscosity measurement value is recorded to reflect the viscosity of the blended material.
SCOPE
1.1 The use of high-viscosity asphalt binders like asphalt-rubber is becoming more common in the United States and worldwide. Specifications such as Specification D6114/D6114M note the need for field control of the apparent viscosity and require the use of a field production rotational viscometer. The testing of asphalt-rubber binder for use in asphalt-rubber hot mix and for asphalt-rubber membrane is necessary to ensure consistent mix properties that will ensure good performance of these materials. Logistics of field applications limits the use of conventional laboratory controls and testing equipment. This test, using a handheld rotational viscometer, can be conducted in either the field or laboratory to determine the apparent viscosity of asphalt-rubber and other high-viscosity binders for field production control and to assess the uniformity of the binder produced, or for other related purposes.  
1.2 Asphalt-rubber binder consists of a blend of paving grade asphalt cement and crumb rubber as described in Specification D6114/D6114M. Other high-viscosity asphalt binders may consist of asphalts modified with polymer or fiber, or both. Testing is performed following the specified reaction time, if any, within the production process. Control of the raw materials is separate from the test.  
1.3 The values stated in SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; each system shall be used independently of the other. Combining values from the two systems may result in noncompliance with the standard.  
1.4 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 The float test characterizes the flow behavior or consistency of certain asphalt materials.  
4.2 This test method is useful in determining the consistency of asphalt as one element in establishing the uniformity of certain shipments or sources of supply.
Note 1: The quality of results produced by this standard is dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guidance provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method covers the float test for asphalt materials.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 Warning—Mercury has been designated by EPA and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Material Safety Data Sheet (MSDS) for details and EPA’s website (http://www.epa.gov/mercury/faq.htm) for additional information. Users should be aware that selling mercury or mercury-containing products, or both, in your state may be prohibited by state law.  
1.4 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 The viscosity at 60 °C [140 °F] characterizes flow behavior and may be used for specification requirements for cutback asphalt and asphalt binders.
Note 3: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method covers procedures for the determination of the apparent viscosity of asphalt binder by vacuum capillary viscometers at 60 °C [140 °F]. It is applicable to materials having viscosities in the range from 0.0036 to over 20 000 Pa·s [0.036 to over 200 000 P].  
Note 1: This test method is suitable for use at other temperatures, but the precision is based on determinations on asphalt binders at 60 °C [140 °F].
Note 2: Modified asphalt binders or asphalt binders that have been conditioned or recovered are typically non-Newtonian under the conditions of this test. The apparent viscosity for non-Newtonian asphalt binders varies with shear rate. When the flow is non-Newtonian in a capillary tube, the shear rate determined using this test method may be invalid. The presence of non-Newtonian behavior for the test conditions of this test can be verified by measuring the viscosity with viscometers having different-sized capillary tubes or with different pressure heads. The defined precision limits in Section 11 may not be applicable to non-Newtonian asphalt binders. Test Method D4957 may be a more applicable method for testing non-Newtonian asphalts.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency (EPA) and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Material Safety Data Sheet (MSDS) or Safety Data Sheet (SDS) for details and the EPA’s website—http://www.epa.gov/mercury/faq.htm—for additional information. Users should be aware that selling mercury, mercury-containing products, or both, in your state may be prohibited by state law.  
1.4 The text of this standard references notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 The continuous grading temperatures and continuous grade are used for informational purposes only and shall not be used for the sale or purchase of asphalt binders. The continuous grading temperatures and continuous grade may be used for forensic or research studies and when producing, blending, modifying, or otherwise evaluating asphalt binders. This guide is applicable to Specification D6373, Tables 1 and 2.
Note 1: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This practice is used to estimate the continuous grading temperatures and continuous grade for an asphalt binder graded in accordance with the requirements specified in Specification D6373.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 This test method is useful in confirming that a material has been added to the asphalt to provide a significant elastomeric characteristic. It does not necessarily identify the type or amount of material added.
Note 1: The quality of results produced by this standard is dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guidance provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method assesses the elastic recovery of an asphalt material measured by the recoverable strain determined after severing an elongated briquet specimen of the material of the form described in 4.1. The specimens are pulled to a specified distance at a specified speed and at a specified temperature. Unless otherwise specified, the test shall be made at a temperature of 25 ± 0.5 °C [77 ± 0.9 °F] and with a speed of 5 cm/min ± 5 %.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable Material Safety Data Sheet (MSDS) for details and EPA’s website (http://www.epa.gov/mercury/index.htm) for additional information. Users should be aware that selling mercury and/or mercury-containing products in your state may be prohibited by state law.  
1.4 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 The penetration test is used as a measure of consistency. Higher values of penetration indicate softer consistency.
Note 2: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method covers determination of the penetration of semi-solid and solid bituminous materials.  
1.2 The needles, containers, and other conditions described in this test method provide for the determinations of penetrations up to 500.
Note 1: See the section on Penetration of Test Methods D244 for information and precision and bias on testing emulsion residue.  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.4 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 This test method is used to identify the presence of elastic response in a binder and the change in elastic response at two different stress levels. Non-recoverable creep compliance has been shown to be an indicator of the resistance of an asphalt binder to permanent deformation under repeated load.  
5.2 This test method is also useful as a surrogate for other test methods used to measure elasticity in asphalt binders such as Test Method D5801 (toughness and tenacity), Test Method D6084/D6084M (elastic recovery), and Test Method D7175 (DSR phase angle).
Note 2: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method covers the determination of percent recovery and non-recoverable creep compliance of asphalt binders by means of multiple stress creep and recovery (MSCR) testing. The MSCR test is conducted using the dynamic shear rheometer (DSR) at a specified temperature.  
1.2 This standard is appropriate for unaged material, material aged in accordance with Test Method D2872 (RTFOT), material aged in accordance with Practice D6521 (PAV), and material aged in accordance with both Test Method D2872 and Practice D6521.
Note 1: The majority of development work on this test method was performed on material aged in accordance with Test Method D2872 (RTFOT).  
1.3 The percent recovery is intended to provide a means to determine the presence of elastic response and stress dependence of polymer-modified and unmodified asphalt binders.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 This test method is useful for characterizing the flow behavior of asphalt emulsion residues and non-Newtonian asphalts. However, since non-Newtonian viscosity values depend on the level of shearing stress, its duration, and the shear history of the material, a non-Newtonian viscosity is not a unique material property. Instead, it is a parameter which is characteristic of the fluid-viscometer system under the conditions of the measurement procedure. Therefore, comparisons of non-Newtonian material behavior should only be made using apparent viscosities determined in similar viscometers under similar conditions of shearing stress and stress history. Procedures of sample preparation are especially important for repeatability or reproducibility of test results.
Note 3: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capacity, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method describes procedures primarily designed to determine the apparent viscosities of residues obtained by distilling asphalt emulsions according to Test Method D6997. It is also recommended for use on non-Newtonian asphalts at any temperature within the capability of the apparatus. This test method is useful in characterizing rheological properties of non-Newtonian asphalts as a function of shear rate under the conditions of the test method. This test is run in straight open-end tube viscometers, normally at 60 °C, but is suitable for use at other temperatures. It is applicable over the range from 5 to 50 000 Pa·s.  
Note 1: The precision for this test method is based on determinations made at 60 °C.  
1.2 The values stated in SI units are to be regarded as the standard, except in reference to viscometer constant or calibration factor (K).  
1.3 Warning— Mercury has been designated by the United States Environmental Protection Agency (EPA) and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury or its vapor may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Material Safety Data Sheets (MSDS) for details and the EPA’s website (www.epa.gov/mercury/faq.htm) for additional information. Users should be aware that selling mercury, mercury-containing products, or both, in your state may be prohibited by state law.  
1.4 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 This test method provides one measure of tensile properties of asphalt materials and may be used to measure ductility for specification requirements.
Note 1: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method describes the procedure for determining the ductility of an asphalt material measured by the distance to which it will elongate before breaking when two ends of a briquet specimen of the material of the form described in 4.1 are pulled apart at a specified speed and at a specified temperature. Unless otherwise specified, the test shall be made at a temperature of 25 ± 0.5 °C [77 ± 0.9 °F] and with a speed of 5 cm/min ± 5.0 %. At other temperatures the speed should be specified.  
1.2 Because of the large number of methods for obtaining test samples, it is impractical to discuss specific products in this test method. Refer to individual product specifications for guidance in obtaining a test sample.  
1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.4 The values stated in SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of each other. Combining values from the two systems may result in nonconformance with the standard. Bath and mold dimensions are given in SI units only, as the equipment is not available in inch-pound units.  
1.5 Warning—Mercury has been designated by the United States Environmental Protection Agency and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury or its vapor may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for details and the EPA’s website (http://www.epa.gov/mercury/faq.htm) for additional information. Users should be aware that selling mercury or mercury-containing products, or both, in your state may be prohibited by state law.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SCOPE
1.1 The viscosity-temperature chart covered by this standard is a convenient means of plotting data for estimating the viscosity of asphalt binders at any temperature within a limited range. Conversely, the chart may be used to ascertain the temperature at which a desired viscosity is attained.  
1.2 The chart is suitable for asphalt binders and for asphalts recovered from laboratory aging tests or extracted from pavements.  
1.3 The chart is based on a viscosity-temperature relationship that can be plotted using any appropriate set of units. For convenience, charts based on both conventional and SI units are provided.  
1.4 The range of the chart is sufficient for roofing asphalts.  
1.5 The range of the chart is sufficient for asphalt binders whose viscosity exceeds 0.01 Pa.S (10 centipoise).  
1.6 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.

SIGNIFICANCE AND USE
5.1 The temperatures for this test are based upon the winter temperature experienced by the pavement in the geographical area for which the asphalt binder is intended.  
5.2 The flexural creep stiffness or flexural creep compliance, determined from this test, describes the low-temperature stress-strain-time response of asphalt binder at the test temperature within the range of linear viscoelastic response.  
5.3 The low-temperature thermal cracking performance of asphalt pavements is related to the creep stiffness and the m-value of the asphalt binder contained in the mix.  
5.4 The creep stiffness and the m-value are used as performance-based specification criteria for asphalt binders in accordance with Specification D6373.
SCOPE
1.1 This test method covers the determination of the flexural-creep stiffness or compliance and m-value of asphalt binders by means of a bending beam rheometer. It is applicable to material having flexural-creep stiffness values in the range of 20 MPa to 1 GPa (creep compliance values in the range of 50 nPa–1 to 1 nPa–1) and can be used with unaged material or with materials aged using aging procedures such as Test Method D2872 or Practice D6521. The test apparatus may be operated within the temperature range from –36°C to 0°C.  
1.2 Test results are not valid for test specimens that deflect more than 4 mm or less than 0.08 mm when tested in accordance with this test method.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
5.1 The kinematic viscosity characterizes flow behavior. The method is used to determine the consistency of liquid asphalt as one element in establishing the uniformity of shipments or sources of supply. The specifications are usually at temperatures of 60 and 135 °C.
Note 3: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method covers procedures for the determination of kinematic viscosity of liquid asphalts, road oils, and distillation residues of liquid asphalts all at 60 °C [140 °F] and of liquid asphalt binders at 135 °C [275 °F] (see table notes, 11.1) in the range from 6 to 100 000 mm2/s [cSt].  
1.2 Results of this test method can be used to calculate viscosity when the density of the test material at the test temperature is known or can be determined. See Annex A1 for the method of calculation.  
Note 1: This test method is suitable for use at other temperatures and at lower kinematic viscosities, but the precision is based on determinations on liquid asphalts and road oils at 60 °C [140 °F] and on asphalt binders at 135 °C [275 °F] only in the viscosity range from 30 to 6000 mm2/s [cSt].
Note 2: Modified asphalt binders or asphalt binders that have been conditioned or recovered are typically non-Newtonian under the conditions of this test. The viscosity determined from this method is under the assumption that asphalt binders behave as Newtonian fluids under the conditions of this test. When the flow is non-Newtonian in a capillary tube, the shear rate determined by this method may be invalid. The presence of non-Newtonian behavior for the test conditions can be verified by measuring the viscosity with viscometers having different-sized capillary tubes. The defined precision limits in 11.1 may not be applicable to non-Newtonian asphalt binders.  
1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency (EPA) and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Material Safety Data Sheet (MSDS) or Safety Data Sheet (SDS) for details and the EPA’s website—http://www.epa.gov/mercury/faq.htm—for additional information. Users should be aware that selling mercury, mercury-containing products, or both, in your state may be prohibited by state law.  
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.5 The text of this standard references notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior ...

SIGNIFICANCE AND USE
5.1 The penetration test is used as a measure of consistency. Higher values of penetration indicate softer consistency.
Note 2: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method covers determination of the penetration of semi-solid and solid bituminous materials.  
1.2 The needles, containers, and other conditions described in this test method provide for the determinations of penetrations up to 500.
Note 1: See the section on Penetration of Test Methods D244 for information and precision and bias on testing emulsion residue.  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.4 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 The penetration test is used as a measure of consistency. Higher values of penetration indicate softer consistency.
Note 2: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method covers determination of the penetration of semi-solid and solid bituminous materials.  
1.2 The needles, containers, and other conditions described in this test method provide for the determinations of penetrations up to 500.
Note 1: See the section on Penetration of Test Methods D244 for information and precision and bias on testing emulsion residue.  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.4 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 The viscosity at 60 °C [140 °F] characterizes flow behavior and may be used for specification requirements for cutback asphalt and asphalt binders.
Note 3: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method covers procedures for the determination of the apparent viscosity of asphalt binder by vacuum capillary viscometers at 60 °C [140 °F]. It is applicable to materials having viscosities in the range from 0.0036 to over 20 000 Pa·s [0.036 to over 200 000 P].  
Note 1: This test method is suitable for use at other temperatures, but the precision is based on determinations on asphalt binders at 60 °C [140 °F].
Note 2: Modified asphalt binders or asphalt binders that have been conditioned or recovered are typically non-Newtonian under the conditions of this test. The apparent viscosity for non-Newtonian asphalt binders varies with shear rate. When the flow is non-Newtonian in a capillary tube, the shear rate determined using this test method may be invalid. The presence of non-Newtonian behavior for the test conditions of this test can be verified by measuring the viscosity with viscometers having different-sized capillary tubes or with different pressure heads. The defined precision limits in Section 11 may not be applicable to non-Newtonian asphalt binders. Test Method D4957 may be a more applicable method for testing non-Newtonian asphalts.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency (EPA) and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Material Safety Data Sheet (MSDS) or Safety Data Sheet (SDS) for details and the EPA’s website—http://www.epa.gov/mercury/faq.htm—for additional information. Users should be aware that selling mercury, mercury-containing products, or both, in your state may be prohibited by state law.  
1.4 The text of this standard references notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 The kinematic viscosity characterizes flow behavior. The method is used to determine the consistency of liquid asphalt as one element in establishing the uniformity of shipments or sources of supply. The specifications are usually at temperatures of 60 and 135 °C.
Note 3: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method covers procedures for the determination of kinematic viscosity of liquid asphalts, road oils, and distillation residues of liquid asphalts all at 60 °C [140 °F] and of liquid asphalt binders at 135 °C [275 °F] (see table note, 11.1) in the range from 6 to 100 000 mm2/s [cSt].  
1.2 Results of this test method can be used to calculate viscosity when the density of the test material at the test temperature is known or can be determined. See Annex A1 for the method of calculation.  
Note 1: This test method is suitable for use at other temperatures and at lower kinematic viscosities, but the precision is based on determinations on liquid asphalts and road oils at 60 °C [140 °F] and on asphalt binders at 135 °C [275 °F] only in the viscosity range from 30 to 6000 mm2/s [cSt].
Note 2: Modified asphalt binders or asphalt binders that have been conditioned or recovered are typically non-Newtonian under the conditions of this test. The viscosity determined from this method is under the assumption that asphalt binders behave as Newtonian fluids under the conditions of this test. When the flow is non-Newtonian in a capillary tube, the shear rate determined by this method may be invalid. The presence of non-Newtonian behavior for the test conditions can be verified by measuring the viscosity with viscometers having different-sized capillary tubes. The defined precision limits in 11.1 may not be applicable to non-Newtonian asphalt binders.  
1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency (EPA) and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Material Safety Data Sheet (MSDS) or Safety Data Sheet (SDS) for details and the EPA’s website—http://www.epa.gov/mercury/faq.htm—for additional information. Users should be aware that selling mercury, mercury-containing products, or both, in your state may be prohibited by state law.  
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.  
1.5 The text of this standard references notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior ...

SIGNIFICANCE AND USE
3.1 This test method is useful in confirming that a material has been added to the asphalt to provide a significant elastomeric characteristic. It does not necessarily identify the type or amount of material added.
Note 1: The quality of results produced by this standard is dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guidance provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method assesses the elastic recovery of an asphalt material measured by the recoverable strain determined after severing an elongated briquet specimen of the material of the form described in 4.1. The specimens are pulled to a specified distance at a specified speed and at a specified temperature. Unless otherwise specified, the test shall be made at a temperature of 25 ± 0.5 °C [77 ± 0.9 °F] and with a speed of 5 cm/min ± 5 %.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.  
1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable Material Safety Data Sheet (MSDS) for details and EPA’s website (http://www.epa.gov/mercury/index.htm) for additional information. Users should be aware that selling mercury and/or mercury-containing products in your state may be prohibited by state law.  
1.4 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 This test is primarily used for field production control of asphalt-rubber (A-R) and other high-viscosity binders; however, the test can also be used in a laboratory setting.  
3.2 A handheld rotational viscometer is used to measure the apparent viscosity of a completed blend of A-R or high-viscosity binder. A rotor (spindle), turning at constant speed, is inserted in the liquid binder to be measured. The resistance to movement of the spindle (torque) caused by the viscosity of the surrounding liquid is measured using a special mechanism to obtain direct readings in Pa·s or cP.
Note 1: Spindle is generally made of stainless steel, although another metal such as brass could be used.  
3.3 The measured apparent viscosity is used to control the production of the A-R or other high-viscosity binder, to assess the uniformity of the binder produced, or for other related purposes.  
3.4 As the spindle turns in the A-R or other high-viscosity binder, it has a tendency to “drill” into the sample (that is, for A-R, the spindle spins the rubber particles out of the measurement area). Consequently, the apparent viscosity drops to reflect only the liquid phase of the high-viscosity binder. Therefore, the peak viscosity measurement value is recorded to reflect the viscosity of the blended material.
SCOPE
1.1 The use of high-viscosity asphalt binders like asphalt-rubber is becoming more common in the United States and worldwide. Specifications such as Specification D6114 note the need for field control of the apparent viscosity and require the use of a field production rotational viscometer. The testing of asphalt-rubber binder for use in asphalt-rubber hot mix and for asphalt-rubber membrane is necessary to ensure consistent mix properties that will ensure good performance of these materials. Logistics of field applications limits the use of conventional laboratory controls and testing equipment. This test, using a handheld rotational viscometer, can be conducted in either the field or laboratory to determine the apparent viscosity of asphalt-rubber and other high-viscosity binders for field production control and to assess the uniformity of the binder produced, or for other related purposes.  
1.2 Asphalt-rubber binder consists of a blend of paving grade asphalt cement and crumb rubber as described in Specification D6114. Other high-viscosity asphalt binders may consist of asphalts modified with polymer or fiber, or both. Testing is performed following the specified reaction time, if any, within the production process. Control of the raw materials is separate from the test.  
1.3 The values stated in SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; each system shall be used independently of the other. Combining values from the two systems may result in noncompliance with the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 This test method provides one measure of tensile properties of asphalt materials and may be used to measure ductility for specification requirements.
Note 1: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method describes the procedure for determining the ductility of an asphalt material measured by the distance to which it will elongate before breaking when two ends of a briquet specimen of the material, of the form described in 4.1, are pulled apart at a specified speed and at a specified temperature. Unless otherwise specified, the test shall be made at a temperature of 25 ± 0.5 °C [77 ± 0.9 °F] and with a speed of 5 cm/min ± 5.0 %. At other temperatures the speed should be specified.  
1.2 Because of the large number of methods for obtaining test samples, it is impractical to discuss specific products in this test method. Refer to individual product specifications for guidance in obtaining a test sample.  
1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.4 The values stated in SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of each other. Combining values from the two systems may result in nonconformance with the standard. Bath and mold dimensions are given in SI units only, as the equipment is not available in inch-pound units.  
1.5 Warning—Mercury has been designated by the United States Environmental Protection Agency and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury or its vapor may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for details and the EPA’s website (http://www.epa.gov/mercury/faq.htm) for additional information. Users should be aware that selling mercury or mercury-containing products, or both, in your state may be prohibited by state law.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 This test is primarily used for field production control of asphalt-rubber (A-R) and other high-viscosity binders; however, the test can also be used in a laboratory setting.  
3.2 A handheld rotational viscometer is used to measure the apparent viscosity of a completed blend of A-R or high-viscosity binder. A rotor (spindle), turning at constant speed, is inserted in the liquid binder to be measured. The resistance to movement of the spindle (torque) caused by the viscosity of the surrounding liquid is measured using a special mechanism to obtain direct readings in Pa·s or cP.
Note 1: Spindle generally made of stainless steel, although another metal such as brass could be used.  
3.3 The measured apparent viscosity is used to control the production of the A-R or other high-viscosity binder, to assess the uniformity of the binder produced or for other related purposes.  
3.4 As the spindle turns in the A-R or other high-viscosity binder, it has a tendency to “drill” into the sample (i.e., for A-R, the spindle spins the rubber particles out of the measurement area). Consequently, the apparent viscosity drops to reflect only the liquid phase of the high-viscosity binder. Therefore, the peak viscosity measurement value is recorded to reflect the viscosity of the blended material.
SCOPE
1.1 The use of high-viscosity asphalt binders like asphalt-rubber is becoming more common in the United States and worldwide. Specifications such as Specification D6114 note the need for field control of the apparent viscosity and require the use of a field production rotational viscometer. The testing of asphalt-rubber binder for use in asphalt-rubber hot mix and for asphalt-rubber membrane is necessary to ensure consistent mix properties that will ensure good performance of these materials. Logistics of field applications limits the use of conventional laboratory controls and testing equipment. This test, using a handheld rotational viscometer can be conducted in either the field or laboratory to determine the apparent viscosity of asphalt-rubber and other high-viscosity binders for field production control and to assess the uniformity of the binder produced or for other related purposes.  
1.2 Asphalt-rubber binder consists of a blend of paving grade asphalt cement and crumb rubber as described in Specification D6114. Other high-viscosity asphalt binders may consist of asphalts modified with polymer or fiber, or both. Testing is performed following the specified reaction time, if any, within the production process. Control of the raw materials is separate from the test.  
1.3 The values stated in SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; each system shall be used independently of the other. Combining values from the two systems may result in noncompliance with the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 This test method is useful in confirming that an asphalt cement has been modified with a material that provides a significant elastomeric component. Elastomer-modified asphalts can be characterized by their ability to be stretched to a large elongation while at the same time resisting further stretching. Toughness and tenacity are two parameters for measuring this ability.
Note 1: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors: following the suggestions of Specification D3666 and or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method describes the procedure for measuring the toughness and tenacity of asphalt materials. Typically, the test method has been used to characterize elastomer modified asphalts, although values for toughness and tenacity may be obtained for any type of polymer-modified or non-modified asphalt.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.2.1 Exception—Sample mass is given only in SI units. Sample mass as given in SI units should be regarded as standard. No other units of sample mass are included in this standard.  
1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable Material Safety Data Sheet (MSDS) for details and EPA’s website – http://www.epa.gov/mercury/index.htm – for additional information. Users should be aware that selling mercury and/or mercury-containing products in your state may be prohibited by state law.  
1.4 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
This test method is useful for characterizing the flow behavior of asphalt emulsion residues and non-Newtonian bitumens. However, since non-Newtonian viscosity values depend on the level of shearing stress, its duration, and the shear history of the material, a non-Newtonian viscosity is not a unique material property. Instead, it is a parameter which is characteristic of the fluid-viscometer system under the conditions of the measurement procedure. Therefore, comparisons of non-Newtonian material behavior should only be made using apparent viscosities determined in similar viscometers under similar conditions of shearing stress and stress history. Procedures of sample preparation are especially important for repeatability or reproducibility of test results.
SCOPE
1.1 This test method describes procedures primarily designed to determine the apparent viscosities of residues obtained by distilling asphalt emulsions according to Test Method D 6997`. It is also recommended for use on non-Newtonian asphalts at any temperature within the capability of the apparatus. This test method is useful in characterizing rheological properties of non-Newtonian bitumens as a function of shear rate under the conditions of the test method. This test is run in straight open-end tube viscometers, normally at 60°C (140°F), but is suitable for use at other temperatures. It is applicable over the range from 5 to 50 000 Pa·s (50 to 500 000 P).
Note 1—The precision for this test method is based on determinations made at 60°C (140°F).  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
WITHDRAWN RATIONALE
This test method described procedures primarily designed to determine the apparent viscosities of residues obtained by distilling asphalt emulsions according to Test Method D6997.
Formerly under the jurisdiction of Committee D04 on Road and Paving Materials, this test method was withdrawn in January 2017 in accordance with section 10.5.3.1 of the Regulations Governing ASTM Technical Committees, which requires that standards shall be updated by the end of the eighth year since the last approval date.

SIGNIFICANCE AND USE
5.1 Estimated critical cracking temperature, as determined by this practice, is a criterion for specifying the low-temperature properties of asphalt binder in accordance with Specification D6373.  
5.2 This practice is designed to identify the temperature region where the induced thermal stress in a typical HMA subjected to rapid cooling (1 °C/h) exceeds the fracture stress of the HMA.  
5.3 For evaluating an asphalt binder for conformance to Specification D6373, the test temperature for the BBR and DTT data is selected from Table 1 of Specification D6373 according to the grade of asphalt binder.
Note 3: Other rates of elongation and test temperatures may be used to test asphalt binders for research purposes.
SCOPE
1.1 This practice covers the calculation of low-temperature properties of asphalt binders using data from the bending beam rheometer (see Test Method D6648) (BBR) and the direct tension tester (see Test Method D6723) (DTT). It can be used on data from unaged material or from material aged using Test Method D2872 (RTFOT), Practice D6521 (PAV), or Test Method D2872 (RTFOT) and Practice D6521 (PAV). It can be used on data generated within the temperature range from +6 °C to –36 °C. This practice generates data suitable for use in binder specifications such as Specification D6373.  
1.2 This practice is only valid for data on materials that fall within the scope of suitability for both Test Method D6648 and Test Method D6723.  
1.3 This practice can be used to determine the following:  
1.3.1 Critical cracking temperature of an asphalt binder, and  
1.3.2 Whether or not the failure stress exceeds the thermal stress in a binder at a given temperature.  
1.4 This practice determines the critical cracking temperature for a typical asphalt binder based on the determination of the temperature where the asphalt binder's strength equals its thermal stress as calculated by this practice. The temperature so determined is intended to yield a low temperature PG Grade of the sample being tested. The low temperature PG grade is intended for use in purchase specifications and is not intended to be a performance prediction of the HMA (Hot Mix Asphalt) in which the asphalt binder is used.  
1.5 The development of this standard was based on SI units. In cases where units have been omitted, SI units are implied.  
1.6 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Note 1: The algorithms contained in this standard require implementation by a person trained in the subject of numerical methods and viscoelasticity. However, due to the complexity of the calculations they must, of necessity, be performed on a computer. Software to perform the calculation may be written, purchased as a spreadsheet, or as a stand-alone program.2

SIGNIFICANCE AND USE
5.1 The continuous grading temperatures and continuous grade are used for informational purposes only and shall not be used for the sale or purchase of asphalt binders. The continuous grading temperatures and continuous grade may be used for forensic or research studies and when producing, blending, modifying, or otherwise evaluating asphalt binders. This guide is applicable to Specification D6373, Tables 1 and 2.
SCOPE
1.1 This practice is used to estimate the continuous grading temperatures and continuous grade for an asphalt binder graded in accordance with the requirements specified in Specification D6373.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
4.1 The float test characterizes the flow behavior or consistency of certain bituminous materials.  
4.2 This test method is useful in determining the consistency of bitumen as one element in establishing the uniformity of certain shipments or sources of supply.
SCOPE
1.1 This test method covers the float test for bituminous materials.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 Warning—Mercury has been designated by EPA and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Material Safety Data Sheet (MSDS) for details and EPA’s website (http://www.epa.gov/mercury/faq.htm) for additional information. Users should be aware that selling mercury or mercury-containing products, or both, in your state may be prohibited by state law.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For a specific precaution statement, see 6.1.

SIGNIFICANCE AND USE
This test method provides one measure of tensile properties of bituminous materials and may be used to measure ductility for specification requirements.
SCOPE
1.1 This test method describes the procedure for determining the ductility of a bituminous material measured by the distance to which it will elongate before breaking when two ends of a briquet specimen of the material, of the form described in Section 4, are pulled apart at a specified speed and at a specified temperature. Unless otherwise specified, the test shall be made at a temperature of 25 ± 0.5°C and with a speed of 5 cm/min ± 5.0 %. At other temperatures the speed should be specified.
1.2 Because of the large number of methods for obtaining test samples, it is impractical to discuss specific products in this test method. Refer to individual product specifications for guidance in obtaining a test sample.
1.3 The values stated in SI units are to be regarded as the standard. Values in parenthesis in inch-pound units are provided for informational purposes only.
1.4 Warning—Mercury has been designated by EPA and many state agencies as a hazardous material that can cause central nervous system, kidney and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable product Material Safety Data Sheet (MSDS) for details and EPA’s website (http://www.epa.gov/mercury/faq.htm) for additional information. Users should be aware that selling mercury or mercury containing products, or both, in your state may be prohibited by state law.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
WITHDRAWN RATIONALE
This test method describes the procedure for determining the ductility of a bituminous material measured by the distance to which it will elongate before breaking when two ends of a briquet specimen of the material are pulled apart at a specified speed and at a specified temperature.
Formerly under the jurisdiction of Committee D04 on Road and Paving Materials, this test method was withdrawn in January 2016 in accordance with section 10.6.3 of the Regulations Governing ASTM Technical Committees, which requires that standards shall be updated by the end of the eighth year since the last approval date.

SIGNIFICANCE AND USE
5.1 This test method is used to identify the presence of elastic response in a binder and the change in elastic response at two different stress levels. Non-recoverable creep compliance has been shown to be an indicator of the resistance of an asphalt binder to permanent deformation under repeated load.  
5.2 This test method is also useful as a surrogate for other test methods used to measure elasticity in asphalt binders such as Test Method D5801 (Toughness and Tenacity), Test Method D6084 (Elastic Recovery), and Test Method D7175 (DSR phase angle).
SCOPE
1.1 This test method covers the determination of percent recovery and non-recoverable creep compliance of asphalt binders by means of Multiple Stress Creep and Recovery (MSCR) testing. The MSCR test is conducted using the Dynamic Shear Rheometer (DSR) at a specified temperature.  
1.2 This standard is appropriate for unaged material, material aged in accordance with Test Method D2872 (RTFO), material aged in accordance with Practice D6521 (PAV), and material aged in accordance with both Test Method D2872 and Practice D6521.
Note 1: The majority of development work on this test method was performed on material aged in accordance with Test Method D2872 (RTFO).  
1.3 The percent recovery is intended to provide a means to determine the presence of elastic response and stress dependence of polymer modified and unmodified asphalt binders.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
5.1 The test temperature for this test is related to the temperature experienced by the pavement in the geographical area for which the asphalt binder is intended to be used.  
5.2 The complex shear modulus is an indicator of the stiffness or resistance of asphalt binder to deformation under load. The complex shear modulus and the phase angle define the resistance to shear deformation of the asphalt binder in the linear viscoelastic region. The complex modulus and the phase angle are used to calculate performance-related criteria in accordance with Specification D6373 or AASHTO Standard M320.
SCOPE
1.1 This test method covers the determination of the dynamic shear modulus and phase angle of asphalt binders when tested in dynamic (oscillatory) shear using parallel plate geometry. It is applicable to asphalt binders having dynamic shear modulus values in the range from 100 Pa to 10 MPa. This range in modulus is typically obtained between 4 and 88°C at 10 rad/s. This test method is intended for determining the linear viscoelastic properties of asphalt binders as required for specification testing and is not intended as a comprehensive procedure for the full characterization of the viscoelastic properties of asphalt binders.  
1.2 This standard is appropriate for unaged materials, material aged in accordance with Test Method D2872, material aged in accordance with Practice D6521, or material aged in accordance with both Test Method D2872 and Practice D6521. This procedure is limited to asphalt binders that contain particles with largest dimension less than 250 μm.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
3.1 This test method is useful in confirming that a material has been added to the asphalt to provide a significant elastomeric characteristic. It does not necessarily identify the type or amount of material added.
SCOPE
1.1 This test method assesses the elastic recovery of an asphalt material measured by the recoverable strain determined after severing an elongated briquet specimen of the material of the form described in 4.1. The specimens are pulled to a specified distance at a specified speed and at a specified temperature. Unless otherwise specified, the test shall be made at a temperature of 25 ± 0.5°C [77 ± 0.9°F] and with a speed of 5 cm/min ± 5 %.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.  
1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency and many state agencies as a hazardous material that can cause central nervous system, kidney and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable Material Safety Data Sheet (MSDS) for details and EPA’s website (http://www.epa.gov/mercury/index.htm) for additional information. Users should be aware that selling mercury and/or mercury containing products into your state may be prohibited by state law.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
5.1 The penetration test is used as a measure of consistency. Higher values of penetration indicate softer consistency.
SCOPE
1.1 This test method covers determination of the penetration of semi-solid and solid bituminous materials.  
1.2 The needles, containers and other conditions described in this test method provide for the determinations of penetrations up to 500.Note 1—For guidance in preparing and testing emulsion residue specimens for this test method, please refer to Section 35 of Test Method D244.  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
4.1 The float test characterizes the flow behavior or consistency of certain bituminous materials.  
4.2 This test method is useful in determining the consistency of bitumen as one element in establishing the uniformity of certain shipments or sources of supply.
SCOPE
1.1 This test method covers the float test for bituminous materials.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 Warning—Mercury has been designated by EPA and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Material Safety Data Sheet (MSDS) for details and EPA’s website (http://www.epa.gov/mercury/faq.htm) for additional information. Users should be aware that selling mercury or mercury-containing products, or both, in your state may be prohibited by state law.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For a specific precaution statement, see 6.1.

SIGNIFICANCE AND USE
4.1 This test method is useful in confirming that an asphalt cement has been modified with a material that provides a significant elastomeric component. Elastomer modified asphalts can be characterized by their ability to be stretched to a large elongation while at the same time resisting further stretching. Toughness and tenacity are two parameters for measuring this ability.
SCOPE
1.1 This test method describes the procedure for measuring the toughness and tenacity of bituminous materials. Typically, the test method has been used to characterize elastomer modified asphalts, although values for toughness and tenacity may be obtained for any type of polymer-modified or non-modified asphalt.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.2.1 Exception—Sample mass is given only in SI units. Sample mass as given in SI units should be regarded as standard. No other units of sample mass are included in this standard.  
1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency and many state agencies as a hazardous material that can cause central nervous system, kidney and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable Material Safety Data Sheet (MSDS) for details and EPA’s website – http://www.epa.gov/mercury/index.htm - for additional information. Users should be aware that selling mercury and/or mercury containing products into your state may be prohibited by state law.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
This test is primarily used for field production control of Asphalt-Rubber (A-R) and other high viscosity binders; however the test can also be used in a laboratory setting.
A hand held rotational viscometer is used to measure the apparent viscosity of a completed blend of A-R or high viscosity binder. A rotor (spindle), turning at constant speed, is inserted in the liquid binder to be measured. The resistance to movement of the spindle (torque) caused by the viscosity of the surrounding liquid is measured using a special mechanism to obtain direct readings in Pa·s or cP.
Note 1—Spindle generally made of stainless steel, although another metal such as brass could be used.
The measured apparent viscosity is used to control the production of the A-R or other high viscosity binder, to assess the uniformity of the binder produced or for other related purposes.
As the spindle turns in the A-R or other high viscosity binder, it has a tendency to “drill” into the sample (i.e., for A-R, the spindle spins the rubber particles out of the measurement area). Consequently, the apparent viscosity drops to reflect only the liquid phase of the high viscosity binder. Therefore, the peak viscosity measurement value is recorded to reflect the viscosity of the blended material.
SCOPE
1.1 The use of high viscosity asphalt binders like Asphalt-Rubber is becoming more common in the United States and worldwide. Specifications such as Specification D6114 note the need for field control of the apparent viscosity and require the use of a field production rotational viscometer. The testing of Asphalt-Rubber Binder for use in Asphalt- Rubber Hot Mix and for Asphalt-Rubber Membrane is necessary to ensure consistent mix properties that will ensure good performance of these materials. Logistics of field applications limits the use of conventional laboratory controls and testing equipment. This test, using a hand held rotational viscometer can be conducted in either the field or laboratory to determine the apparent viscosity of Asphalt-Rubber and other high viscosity binders for field production control and to assess the uniformity of the binder produced or for other related purposes.
1.2 Asphalt-Rubber Binder consists of a blend of paving grade asphalt cement and crumb rubber as described in Specification D6114. Other high viscosity asphalt binders may consist of asphalts modified with polymer or fiber or both. Testing is performed following the specified reaction time, if any, within the production process. Control of the raw materials is separate from the test.
1.3 The values stated in SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; each system shall be used independently of the other. Combining values from the two systems may result in non-compliance with the standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
This test is primarily used for field production control of Asphalt-Rubber (A-R) and other high viscosity binders; however the test can also be used in a laboratory setting.
A hand held rotational viscometer is used to measure the apparent viscosity of a completed blend of A-R or high viscosity binder. A rotor (spindle), turning at constant speed, is inserted in the liquid binder to be measured. The resistance to movement of the spindle (torque) caused by the viscosity of the surrounding liquid is measured using a special mechanism to obtain direct readings in Pa·s or cP.
Note 1—Spindle generally made of stainless steel, although another metal such as brass could be used.
The measured apparent viscosity is used to control the production of the A-R or other high viscosity binder, to assess the uniformity of the binder produced or for other related purposes.
As the spindle turns in the A-R or other high viscosity binder, it has a tendency to “drill” into the sample (i.e., for A-R, the spindle spins the rubber particles out of the measurement area). Consequently, the apparent viscosity drops to reflect only the liquid phase of the high viscosity binder. Therefore, the peak viscosity measurement value is recorded to reflect the viscosity of the blended material.
SCOPE
1.1 The use of high viscosity asphalt binders like Asphalt-Rubber is becoming more common in the United States and worldwide. Specifications such as Specification D6114 note the need for field control of the apparent viscosity and require the use of a field production rotational viscometer. The testing of Asphalt-Rubber Binder for use in Asphalt- Rubber Hot Mix and for Asphalt-Rubber Membrane is necessary to ensure consistent mix properties that will ensure good performance of these materials. Logistics of field applications limits the use of conventional laboratory controls and testing equipment. This test, using a hand held rotational viscometer can be conducted in either the field or laboratory to determine the apparent viscosity of Asphalt-Rubber and other high viscosity binders for field production control and to assess the uniformity of the binder produced or for other related purposes.
1.2 Asphalt-Rubber Binder consists of a blend of paving grade asphalt cement and crumb rubber as described in Specification D6114. Other high viscosity asphalt binders may consist of asphalts modified with polymer or fiber or both. Testing is performed following the specified reaction time, if any, within the production process. Control of the raw materials is separate from the test.
1.3 The values stated in SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; each system shall be used independently of the other. Combining values from the two systems may result in non-compliance with the standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
Estimated critical cracking temperature, as determined by this practice, is a criterion for specifying the low-temperature properties of asphalt binder in accordance with Specification D6373.
This practice is designed to identify the temperature region where the induced thermal stress in a typical HMA subjected to rapid cooling (1°C/h) exceeds the fracture stress of the HMA.
For evaluating an asphalt binder for conformance to Specification D6373, the test temperature for the BBR and DTT data is selected from Table 1 of Specification D6373 according to the grade of asphalt binder.
Note 3—Other rates of elongation and test temperatures may be used to test asphalt binders for research purposes.
SCOPE
1.1 This practice covers the calculation of low-temperature properties of asphalt binders using data from the bending beam rheometer (see Test Method D6648) (BBR) and the direct tension tester (see Test Method D6723) (DTT). It can be used on data from unaged material or from material aged using Test Method D2872 (RTFOT), Practice D6521 (PAV), or Test Method D2872 (RTFOT) and Practice D6521 (PAV). It can be used on data generated within the temperature range from +6°C to -36°C. This practice generates data suitable for use in binder specifications such as Specification D6373.
1.2 This practice is only valid for data on materials that fall within the scope of suitability for both Test Method D6648 and Test Method D6723.
1.3 This practice can be used to determine the following:
1.3.1 Critical cracking temperature of an asphalt binder, and  
1.3.2 Whether or not the failure stress exceeds the thermal stress in a binder at a given temperature.
1.4 This practice determines the critical cracking temperature for a typical asphalt binder based on the determination of the temperature where the asphalt binder's strength equals its thermal stress as calculated by this practice. The temperature so determined is intended to yield a low temperature PG Grade of the sample being tested. The low temperature PG grade is intended for use in purchase specifications and is not intended to be a performance prediction of the HMA (Hot Mix Asphalt) in which the asphalt binder is used.
1.5 The development of this standard was based on SI units. In cases where units have been omitted, SI units are implied.
1.6 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Note 1—The algorithms contained in this standard require implementation by a person trained in the subject of numerical methods and viscoelasticity. However, due to the complexity of the calculations they must, of necessity, be performed on a computer. Software to perform the calculation may be written, purchased as a spreadsheet, or as a stand-alone program.

SIGNIFICANCE AND USE
Estimated critical cracking temperature, as determined by this practice, is a criterion for specifying the low-temperature properties of asphalt binder in accordance with Specification D 6373.
This practice is designed to identify the temperature region where the induced thermal stress in a typical HMA subjected to rapid cooling (1°C/h) exceeds the fracture stress of the HMA.
For evaluating an asphalt binder for conformance to Specification D 6373, the test temperature for the BBR and DTT data is selected from Table 1 of Specification D 6373 according to the grade of asphalt binder.
Note 3—Other rates of elongation and test temperatures may be used to test asphalt binders for research purposes.
SCOPE
1.1 This practice covers the calculation of low-temperature properties of asphalt binders using data from the bending beam rheometer (see Test Method D 6648) (BBR) and the direct tension tester (see Test Method D 6723) (DTT). It can be used on data from unaged material or from material aged using Test Method D 2872 (RTFOT), Practice D 6521 (PAV), or Test Method D 2872 (RTFOT) and Practice D 6521 (PAV). It can be used on data generated within the temperature range from +6C to -36C. This practice generates data suitable for use in binder specifications such as Specification D 6373.
1.2 This practice is only valid for data on materials that fall within the scope of suitability for both Test Method D 6648 and Test Method D 6723.
1.3 This practice can be used to determine the following:
1.3.1 Critical cracking temperature of an asphalt binder, and
1.3.2 Whether or not the failure stress exceeds the thermal stress in a binder at a given temperature.
1.4 This practice determines the critical cracking temperature for a typical asphalt binder based on the determination of the temperature where the asphalt binder's strength equals its thermal stress as calculated by this practice. The temperature so determined is intended to yield a low temperature PG Grade of the sample being tested. The low temperature PG grade is intended for use in purchase specifications and is not intended to be a performance prediction of the HMA (Hot Mix Asphalt) in which the asphalt binder is used.
1.5 The development of this standard was based on SI units. In cases where units have been omitted, SI units are implied.
1.6 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Note 1—The algorithms contained in this standard require implementation by a person trained in the subject of numerical methods and viscoelasticity. However, due to the complexity of the calculations they must, of necessity, be performed on a computer. Software to perform the calculation may be written, purchased as a spreadsheet, or as a stand-alone program.
WITHDRAWN RATIONALE
Formerly under the jurisdiction of Committee D04 on Road and Paving Materials, this Practice was withdrawn in 2011 in accordance with section 10.5.3.1 of the Regulations Governing ASTM Technical Committees, which requires that standards shall be updated by the end of the eighth year since the last approval date.

SIGNIFICANCE AND USE
Stress at failure is used in a mechanistic pavement cracking model to compute critical cracking temperature. The procedure to compute critical cracking temperature is described in Practice D 6521. The critical cracking temperature is then used in specifying the low temperature grade of asphalt binder in accordance with Specification D 6373.
The test method is designed to measure the strength of the asphalt binder at the critical cracking temperature. The asphalt binder has limited ability to resist stress without cracking. In the asphalt binder Specification D 6373, failure stress is used to determine the critical cracking temperature.
For evaluating an asphalt binder for conformance to Specification D 6373, the elongation rate of the gage section is 1.0 mm/min and the test temperature is selected from Table number 1 of Specification D 6373 according to the grade of asphalt binder. Other rates of elongation and test temperatures may be used to test asphalt binders.
SCOPE
1.1 This test method covers the determination of the failure strain and failure stress of asphalt binders by means of a direct tension test. It can be used with unaged material or with material aged using Test Method D 2872 (RTFOT), Practice D 6521 (PAV), or AASHTO T240 (RTFOT) and AASHTO PP1 (PAV). The test apparatus is designed for testing within the temperature range from +6 to -36°C.
1.2 This test method is limited to asphalt binders containing particulate material having dimensions less than 250 μm.
1.3 The values stated in SI units are to be regarded as the standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
WITHDRAWN RATIONALE
Formerly under the jurisdiction of Committee D04 on Road and Paving Materials, this Test Method was withdrawn in 2011 in accordance with section 10.5.3.1 of the Regulations Governing ASTM Technical Committees, which requires that standards shall be updated by the end of the eighth year since the last approval date.

SIGNIFICANCE AND USE
The kinematic viscosity characterizes flow behavior. The method is used to determine the consistency of bitumen as one element in establishing the uniformity of shipments or sources of supply. The specifications are usually at temperatures of 60 and 135°C.
SCOPE
1.1 This test method covers procedures for the determination of kinematic viscosity of liquid asphalts (bitumens), road oils and distillation residues of liquid asphalts (bitumens) all at 60°C [140°F] and of asphalt cements at 135°C [275°F] (Note 1) in the range from 6 to 100 000 mm2/s [cSt].
1.2 Results of this test method can be used to calculate viscosity when the density of the test material at the test temperature is known or can be determined. See Annex A1 for the method of calculation.
Note 1—This test method is suitable for use at other temperatures and at lower kinematic viscosities, but the precision is based on determinations on liquid asphalts and road oils at 60°C [140°F] and on asphalt cements at 135°C [275°F] only in the viscosity range from 30 to 6000 mm2/s [cSt].  
1.3 Warning—Mercury has been designated by United States Environmental Protection Agency (EPA) and many state agencies as a hazardous material that can cause central nervous system, kidney and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable product Material Safety Data Sheet (MSDS) for details and EPA’s websitehttp://www.epa.gov/mercury/faq.htmfor additional information. Users should be aware that selling mercury, mercury containing products, or both, in your state may be prohibited by state law.
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
The viscosity at 60°C [140°F] characterizes flow behavior and may be used for specification requirements for cutbacks and asphalt binders.
SCOPE
1.1 This test method covers procedures for the determination of viscosity of asphalt binder (bitumen) by vacuum capillary viscometers at 60°C [140°F]. It is applicable to materials having viscosities in the range from 0.0036 to over 20 000 Pa · s [0.036 to over 200 000 P].
Note 1—This test method is suitable for use at other temperatures, but the precision is based on determinations on asphalt binders at 60°C [140°F].  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency (EPA) and many state agencies as a hazardous material that can cause central nervous system, kidney and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable product Material Safety Data Sheet (MSDS) for details and EPA’s websitehttp://www.epa.gov/mercury/faq.htmfor additional information. Users should be aware that selling mercury, mercury-containing products, or both, into your state may be prohibited by state law.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
This test method is used to identify the presence of elastic response in a binder and the change in elastic response at two different stress levels. Non-recoverable creep compliance has been shown to be an indicator of the resistance of an asphalt binder to permanent deformation under repeated load.
This test method is also useful as a surrogate for other test methods used to measure elasticity in asphalt binders such as Test Method D5801 (Toughness and Tenacity), Test Method D6084 (Elastic Recovery), and Test Method D7175 (DSR phase angle).
SCOPE
1.1 This test method covers the determination of percent recovery and non-recoverable creep compliance of asphalt binders by means of Multiple Stress Creep and Recovery (MSCR) testing. The MSCR test is conducted using the Dynamic Shear Rheometer (DSR) at a specified temperature.
1.2 This standard is appropriate for unaged material, material aged in accordance with Test Method D2872 (RTFO), material aged in accordance with Practice D6521 (PAV), and material aged in accordance with both Test Method D2872 and Practice D6521.
Note 1—The majority of development work on this test method was performed on material aged in accordance with Test Method D2872 (RTFO).
1.3 The percent recovery is intended to provide a means to determine the presence of elastic response and stress dependence of polymer modified and unmodified asphalt binders.
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
The continuous grading temperatures and continuous grade are used for informational purposes only and are not used for the sale or purchase of asphalt binders. The continuous grading temperatures and continuous grade may be used for forensic or research studies and when producing, blending, modifying, or otherwise evaluating asphalt binders. This guide is applicable to Specification D6373, Tables 1 and 2.
SCOPE
1.1 This practice is used to determine the continuous grading temperatures and continuous grade for an asphalt binder graded in accordance with the specification criteria specified in D6373, Standard Specification for Performance Graded Asphalt Binders.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
This test method is used to identify the presence of elastic response in a binder and the change in elastic response at two different stress levels. Non-recoverable creep compliance has been shown to be an indicator of the resistance of an asphalt binder to permanent deformation under repeated load.
This test method is also useful as a surrogate for other test methods used to measure elasticity in asphalt binders such as Test Method D5801 (Toughness and Tenacity), Test Method D6084 (Elastic Recovery), and Test Method D7175 (DSR phase angle).
SCOPE
1.1 This test method covers the determination of percent recovery and non-recoverable creep compliance of asphalt binders by means of Multiple Stress Creep and Recovery (MSCR) testing. The MSCR test is conducted using the Dynamic Shear Rheometer (DSR) at a specified temperature.
1.2 This standard is appropriate for unaged material, material aged in accordance with Test Method D2872 (RTFO), material aged in accordance with Practice D6521 (PAV), and material aged in accordance with both Test Method D2872 and Practice D6521.
Note 1—The majority of development work on this test method was performed on material aged in accordance with Test Method D2872 (RTFO).
1.3 The percent recovery is intended to provide a means to determine the presence of elastic response and stress dependence of polymer modified and unmodified asphalt binders.
1.4 A precision and bias statement for this standard has not been developed at this time. Therefore, this standard should not be used for acceptance or rejection of a material for purchasing purposes.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SCOPE
1.1 The viscosity-temperature chart covered by this standard is a convenient means of plotting data for estimating the viscosity of asphalts at any temperature within a limited range. Conversely, the chart may be used to ascertain the temperature at which a desired viscosity is attained.  
1.2 The chart is suitable for original asphalt cements and for asphalts recovered from laboratory aging tests or extracted from pavements.  
1.3 The chart is based on a viscosity–temperature relationship that can be plotted using any appropriate set of units. For convenience, charts based on both conventional and SI units are provided.
1.4 The range of the chart is sufficient for roofing asphalts.
1.5 The range of the chart is sufficient for liquid asphalts (bitumens) whose viscosity exceeds 0.01 Pa.S (10 centipoise).
1.6 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.

SIGNIFICANCE AND USE
The test temperature for this test is related to the temperature experienced by the pavement in the geographical area for which the asphalt binder is intended to be used.
The complex shear modulus is an indicator of the stiffness or resistance of asphalt binder to deformation under load. The complex shear modulus and the phase angle define the resistance to shear deformation of the asphalt binder in the linear viscoelastic region. The complex modulus and the phase angle are used to calculate performance-related criteria in accordance with Specification D 6373 or AASHTO Standard M320.
SCOPE
1.1 This test method covers the determination of the dynamic shear modulus and phase angle of asphalt binders when tested in dynamic (oscillatory) shear using parallel plate geometry. It is applicable to asphalt binders having dynamic shear modulus values in the range from 100 Pa to 10 MPa. This range in modulus is typically obtained between 4 and 88°C at 10 rad/s. This test method is intended for determining the linear viscoelastic properties of asphalt binders as required for specification testing and is not intended as a comprehensive procedure for the full characterization of the viscoelastic properties of asphalt binders.
1.2 This standard is appropriate for unaged materials, material aged in accordance with Test Method D 2872, material aged in accordance with Practice D 6521, or material aged in accordance with both Test Method D 2872 and Practice D 6521. This procedure is limited to asphalt binders that contain particles with largest dimension less than 250 μm.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
This test method is used to identify the presence of elastic response in a binder and the change in elastic response at two different stress levels. Non-recoverable creep compliance has been shown to be an indicator of the resistance of an asphalt binder to permanent deformation under repeated load.
This test method is also useful as a surrogate for other test methods used to measure elasticity in asphalt binders such as Test Method D 5801 (Toughness and Tenacity), Test Method D 6084 (Elastic Recovery), and Test Method D 7175 (DSR phase angle).
SCOPE
1.1 This test method covers the determination of percent recovery and non-recoverable creep compliance of asphalt binders by means of Multiple Stress Creep and Recovery (MSCR) testing. The MSCR test is conducted using the Dynamic Shear Rheometer (DSR) at a specified temperature.
1.2 This standard is appropriate for unaged material, material aged in accordance with Test Method D 2872 (RTFO), material aged in accordance with Practice D 6521 (PAV), and material aged in accordance with both Test Method D 2872 and Practice D 6521.
Note 1—The majority of development work on this test method was performed on material aged in accordance with Test Method D 2872 (RTFO).
1.3 The percent recovery is intended to provide a means to determine the presence of elastic response and stress dependence of polymer modified and unmodified asphalt binders.
1.4 A precision and bias statement for this standard has not been developed at this time. Therefore, this standard should not be used for acceptance or rejection of a material for purchasing purposes.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
This test method is used to identify the presence of elastic response in a binder and the change in elastic response at two different stress levels. Non-recoverable creep compliance has been shown to be an indicator of the resistance of an asphalt binder to permanent deformation under repeated load.
This test method is also useful as a surrogate for other test methods used to measure elasticity in asphalt binders such as Test Method D 5801 (Toughness and Tenacity), Test Method D 6084 (Elastic Recovery) and Test Method D 7175 (DSR phase angle).
SCOPE
1.1 This test method covers the determination of percent recovery and non-recoverable creep compliance of asphalt binders by means of Multiple Stress Creep and Recovery (MSCR) testing. The MSCR test is conducted using the Dynamic Shear Rheometer (DSR) at a specified temperature.
1.2 This standard is appropriate for unaged material, material aged in accordance with Test Method D 2872 (RTFO), material aged in accordance with Practice D 6521 (PAV), and material aged in accordance with both Test Method D 2872 and Practice D 6521.
Note 1—The majority of development work on this test method was performed on material aged in accordance with Test Method D 2872 (RTFO).
1.3 The percent recovery is intended to provide a means to determine the presence of elastic response and stress dependence of polymer modified and unmodified asphalt binders.
1.4 A precision and bias statement for this standard has not been developed at this time. Therefore, this standard should not be used for acceptance or rejection of a material for purchasing purposes.
1.5 The values stated in SI units are to be considered standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
The temperatures for this test are based upon the winter temperature experienced by the pavement in the geographical area for which the asphalt binder is intended.
The flexural creep stiffness or flexural creep compliance, determined from this test, describes the low-temperature stress-strain-time response of asphalt binder at the test temperature within the range of linear viscoelastic response.
The low-temperature thermal cracking performance of asphalt pavements is related to the creep stiffness and the m-value of the asphalt binder contained in the mix.
The creep stiffness and the m-value are used as performance-based specification criteria for asphalt binders in accordance with Specification D 6373.
SCOPE
1.1 This test method covers the determination of the flexural-creep stiffness or compliance and m-value of asphalt binders by means of a bending beam rheometer. It is applicable to material having flexural-creep stiffness values in the range of 20 MPa to 1 GPa (creep compliance values in the range of 50 nPa–1 to 1 nPa–1) and can be used with unaged material or with materials aged using aging procedures such as Test Method D 2872 or Practice D 6521. The test apparatus may be operated within the temperature range from –36°C to 0°C.
1.2 Test results are not valid for test specimens that deflect more than 4 mm or less than 0.08 mm when tested in accordance with this test method.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.