ASTM D1353-13(2021)

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D1353 − 13 (Reapproved 2021)
Standard Test Method for
Nonvolatile Matter in Volatile Solvents for Use in Paint,
Varnish, Lacquer, and Related Products
This standard is issued under the fixed designation D1353; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope 2. Referenced Documents
2.1 ASTM Standards:
1.1 This test method covers the determination of the non-
E29 Practice for Using Significant Digits in Test Data to
volatile matter in volatile solvents for use in paint, varnish,
Determine Conformance with Specifications
lacquer, and related products.
E177 Practice for Use of the Terms Precision and Bias in
1.2 The following applies to all specified limits in this
ASTM Test Methods
standard; for purposes of determining conformance with this
E299 Test Method for Trace Amounts of Peroxides In
standard, an observed value or a calculated value shall be
Organic Solvents
rounded off “to the nearest unit” in the last right-hand digit
E691 Practice for Conducting an Interlaboratory Study to
used in expressing the specification limit, in accordance with
Determine the Precision of a Test Method
the rounding-off method of Practice E29.
3. Significance and Use
1.3 The values stated in SI units are to be regarded as
standard. No other units of measurement are included in this 3.1 This test method describes the analytical measurement
of residual matter in solvents that are intended to be 100 %
standard.
volatile at 105 °C 6 5 °C. Volatile solvents are used in the
1.4 For hazard information and guidance, see the supplier’s
manufacture of paint, varnish, lacquer, and other related
Material Safety Data Sheet for materials listed in this test
products, and the presence of any residue may affect the
method.
product quality or efficiency of the process. This test method is
useful in manufacturing control and assessing compliance with
1.5 This standard does not purport to address all of the
specifications.
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
4. Apparatus
priate safety, health, and environmental practices and deter-
mine the applicability of regulatory limitations prior to use.
4.1 Oven, thermostatically controlled at 105 °C 6 5 °C.
For specific hazard statements, see Section 5.
4.2 Dish, evaporating, platinum, 125-mL. A platinum
1.6 This international standard was developed in accor-
evaporating dish is preferred. Alternatively, an aluminum or
dance with internationally recognized principles on standard-
porcelain dish may be used (see Note 1).
ization established in the Decision on Principles for the
NOTE 1—Precision data were determined utilizing only platinum
Development of International Standards, Guides and Recom-
dishes.
mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee.
4.3 Cylinder, graduated, 100-mL.
4.4 Analytical Balance, precision to 60.1 mg.
This test method is under the jurisdiction of ASTM Committee D01 on Paint
and Related Coatings, Materials, andApplications and is the direct responsibility of
Subcommittee D01.35 on Solvents, Plasticizers, and Chemical Intermediates. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved July 1, 2021. Published August 2021. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 1954. Last previous edition approved in 2013 as D1353 – 13. DOI: Standards volume information, refer to the standard’s Document Summary page on
10.1520/D1353-13R21. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D1353 − 13 (2021)
5. Hazards Nonvolatile Matter in Volatile Solvents for Use in Paint,
Varnish, Lacquer, and Related Products, conducted in 2012.
5.1 Warning—Certain solvents and chemical
Eight laboratories participated in the study, testing a single
intermediates, particularly, but not only ethers and unsaturated
material. Every analyst was instructed to report duplicate test
compounds, may form peroxides during storage. These perox-
results in this study. Practice E691 was followed for the study
ides may present a violent explosion hazard when the chemi-
design; the details are given in ASTM Research Report No.
calsareevaporated.Whenperoxideformationislikelybecau
...