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ASTM D3607-97

(Test Method)

Standard Test Method for Removing Volatile Contaminants from Used Engine Oils by Stripping

Standard Test Method for Removing Volatile Contaminants from Used Engine Oils by Stripping

SCOPE
1.1 This test method describes a standardized procedure for removing volatile materials such as gasoline and water from used engine oils prior to further oil analysis. It also provides an estimate of the amount of such volatiles present in used engine oils.  
1.1.1 Another estimate of the amount of volatile materials in used engine oils can be obtained by Test Method D3525, which determines the weight percent of the used oil sample boiling below the boiling point of n-tetradecene. In any case of dispute, the amount of volatiles as determined by Test Method D3525 shall be considered the referee value.  Note 1-The time and temperature conditions specified in this test method have proven adequate for most oils tested for balancing the viscosity effects caused by removal of the heaviest gasoline ends and those caused by the removal of the lightest base oil fractions. Thus at times the test method will slightly overestimate or underestimate the true gasoline content of the oil, especially with oils containing significant amounts of light-base stocks and oils containing abnormally high amounts of heavy gasoline ends.
1.2 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.
1.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to consult and establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statement, see 6.1 and 8.5.

General Information

Status
Historical
Publication Date
09-Dec-1997
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.06.0B - Physical Testing
Current Stage
Ref Project

Relations

Replaced By
ASTM D3607-97(2002)e1 - Standard Test Method for Removing Volatile Contaminants from Used Engine Oils by Stripping
Effective Date
10-Dec-2002

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ASTM D3607-97 - Standard Test Method for Removing Volatile Contaminants from Used Engine Oils by StrippingASTM D3607-97 - Standard Test Method for Removing Volatile Contaminants from Used Engine Oils by Stripping
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ASTM D3607-97 - Standard Test Method for Removing Volatile Contaminants from Used Engine Oils by Stripping
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn. Contact
ASTM International (www.astm.org) for the latest information.
Designation: D 3607 – 97 An American National Standard
AMERICAN SOCIETY FOR TESTING AND MATERIALS
100 Barr Harbor Dr., West Conshohocken, PA 19428
Reprinted from the Annual Book of ASTM Standards. Copyright ASTM
Standard Test Method for
Removing Volatile Contaminants from Used Engine Oils by
1
Stripping
This standard is issued under the fixed designation D 3607; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
4
1. Scope Products, and Lubricants
D 4177 Practice for Automatic Sampling of Petroleum and
1.1 This test method describes a standardized procedure for
3
Petroleum Products
removing volatile materials such as gasoline and water from
5
E 1 Specification for ASTM Thermometers
used engine oils prior to further oil analysis.
1.2 It also provides an estimate of such volatiles in used
3. Terminology
engine oils.
3.1 Definitions:
1.3 When an accurate value of the gasoline contaminant is
3.1.1 stripping, n—the process whereby volatile fractions
required either Test Methods D 322 or D 3525 shall be used.
are removed from a liquid material.
NOTE 1—Test Method D 322 determines the amount of gasoline by
3.1.1.1 Discussion—In this test method, lighter components
distillation with water. Test Method D 3525 determines the amount of
such as water and gasoline are removed by the application of
material boiling below the boiling point of n–tetradecane by gas chroma-
heat while passing an inert gas through the liquid.
tography.
3.1.2 used oil, n—any oil that has been in a piece of
NOTE 2—When the amount of gasoline is required to be known, the
equipment (for example, an engine, gearbox, transformer, or
user of this test method is advised to determine which method is to be
used. There are cases where D 3525 may be set as the referee method. turbine) whether operated or not.
3.1.2.1 Discussion—This test method refers specifically to
1.4 The values stated in SI units are to be regarded as the
used lubricating oils from gasoline engines.
standard. The values in parentheses are for information only.
1.5 This standard does not purport to address all of the
4. Summary of Test Method
safety concerns, if any, associated with its use. It is the
4.1 A known weight of sample is heated to 90°C under a
responsibility of the user of this standard to consult and
nitrogen flow for 4.5 h, cooled, and reweighed.
establish appropriate safety and health practices and deter-
mine the applicability of regulatory limitations prior to use.
5. Significance and Use
For specific precautionary statement, see 6.1 and 8.5.
5.1 The removal of volatile materials such as gasoline
dilution from used engine oils is especially important if the
2. Referenced Documents
mechanical shear stability or oxidative stability of the oil is
2.1 ASTM Standards:
being monitored by measuring a kinematic viscosity change in
D 322 Test Method for Gasoline Diluent in Used Gasoline
2
the oil after it has been used in a gasoline engine.
Engine Oils by Distillation
D 445 Test Method for Kinematic Viscosity of Transparent
6. Apparatus
and Opaque Liquids (and the Calculation of Dynamic
6.1 Nitrogen Cylinder,(Warning—See Note 3), equipped
2
Viscosity)
with regulator.
D 3525 Test Method for Gasoline Diluent in Used Gasoline
3
Engine Oils by Gas Chromatography
NOTE 3—Warning: Using pressurized gas is hazardous.
D 4057 Practice for Manual Sampling of Petroleum and
6
6.2 Rotameters or Nitrogen Flowmeters , one or more, each
3
Petroleum Products
3
capable of supplying 400 cm /min of nitrogen at atmospheric
D 4175 Terminology Relating to Petroleum, Petroleum
pressure.
NOTE 4—If several rotameters are available, it is preferable to control
the nitrogen flow with an individual rotameter to each tube. Consistent
1
flow rates can be maintained to several tubes by one rotameter if the
This test method is under the jurisdiction of ASTM Committee D-2 on
Petroleum Products and Lubricants and is the direct responsibility of Subcommittee
D02.06 on Analysis of Lubricants.
4
Current edition approved Dec. 10, 1997. Published August 1998. Originally Annual Book of ASTM Standards, Vol 05.03.
5
published as D 3607 – 77. Last previous edition D 3607 – 92. Annual Book of ASTM Standards, Vol 14.03.
2 6
Annual Book of ASTM Standards, Vol 05.01. A suitable rotameter is available from Brooks Instrument Co., Inc., Hatfield, PA
3
Annual Book of ASTM Standards, Vol 05.02. 19440, as Sho-Rate 50, Model 1350.
1

---------------------- Page: 1 ----------------------
NOTICE:¬This¬standard¬has¬either¬been¬superceded¬and¬replaced¬by¬a¬new¬version¬or¬discontinued.¬
Contact¬ASTM¬International¬(www.astm.org)¬for¬th
...

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1.1 This specification covers UNS N06002, UNS N06030, UNS N06035, UNS N06022, UNS N06200, UNS N10362, UNS N06230, UNS N06600, UNS N06617, UNS N06625, UNS N08020, UNS N08026, UNS N08024, UNS N08120, UNS N08926, UNS N08367, UNS N10242, UNS N10276, UNS N10665, UNS N10675, UNS N12160, UNS R20033, UNS N06059, UNS N06686, UNS N10629, UNS N08031, UNS N06045, UNS N06025, UNS N06699, and UNS R305562 billets and bars for reforging.  
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