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ASTM D243/D243M-14

(Test Method)

Standard Test Method for Residue of Specified Penetration

Standard Test Method for Residue of Specified Penetration

SIGNIFICANCE AND USE
4.1 This test method is used to determine the percentage of residue having a specified penetration at 100 g/5 s at 25°C [77°F]. This test method provides a residue for quality control or for use in other tests as desired.
SCOPE
1.1 This test method is used to thermally reduce cutback asphalt, a road oil or a semisolid asphalt, having a penetration greater than 100, to a residue of specified penetration. It is primarily used with slow-curing cutback asphalt as specified in Specification D2026.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.  
1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency (EPA) and many state agencies as a hazardous material that can cause central nervous system, kidney and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable product Material Safety Data Sheet (MSDS) for details and EPA’s website—http://www.epa.gov/mercury/—for additional information. Users should be aware that selling mercury, mercury-containing products, or both, into your state may be prohibited by state law.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-May-2014
ICS
93.080.20 - Road construction materials
Technical Committee
D04 - Road and Paving Materials
Drafting Committee
D04.46 - Durability and Distillation Tests
Current Stage
Ref Project

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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D243/D243M −14
Standard Test Method for
1
Residue of Specified Penetration
This standard is issued under the fixed designation D243/D243M; the number immediately following the designation indicates the year
of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval.
A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D2026 Specification for Cutback Asphalt (Slow-Curing
Type)
1.1 This test method is used to thermally reduce cutback
E1 Specification for ASTM Liquid-in-Glass Thermometers
asphalt, a road oil or a semisolid asphalt, having a penetration
E77 Test Method for Inspection and Verification of Ther-
greater than 100, to a residue of specified penetration. It is
mometers
primarily used with slow-curing cutback asphalt as specified in
E220 Test Method for Calibration of Thermocouples By
Specification D2026.
Comparison Techniques
1.2 The values stated in either SI units or inch-pound units
E644 Test Methods for Testing Industrial Resistance Ther-
are to be regarded separately as standard. The values stated in
mometers
each system may not be exact equivalents; therefore, each
E1137/E1137M Specification for Industrial Platinum Resis-
system shall be used independently of the other. Combining
tance Thermometers
values from the two systems may result in non-conformance
with the standard.
3. Summary of Test Method
1.3 Warning—Mercury has been designated by the United
3.1 The material to be tested is rapidly heated to 249°C
States Environmental ProtectionAgency (EPA) and many state
[480°F] and maintained at 249 to 260°C [480 to 500°F] during
agencies as a hazardous material that can cause central nervous
evaporation of the volatiles. Penetration of the residue is
system,kidneyandliverdamage.Mercury,oritsvapor,maybe
determined and if not within the specified limits, the evapora-
hazardous to health and corrosive to materials. Caution should
tion procedure is repeated. Change in sample mass is used to
be taken when handling mercury and mercury containing
calculate the percentage of residue having the specified pen-
products. See the applicable product Material Safety Data
etration.
Sheet (MSDS) for details and EPA’s website—http://
www.epa.gov/mercury/—for additional information. Users
4. Significance and Use
should be aware that selling mercury, mercury-containing
products, or both, into your state may be prohibited by state 4.1 This test method is used to determine the percentage of
law. residue having a specified penetration at 100 g/5 s at 25°C
[77°F]. This test method provides a residue for quality control
1.4 This standard does not purport to address all of the
or for use in other tests as desired.
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
5. Apparatus
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use.
5.1 The apparatus shall consist of a container, heating bath,
hot plate, and thermometric device, with necessary accessory
2. Referenced Documents
apparatus as follows:
2
2.1 ASTM Standards:
5.1.1 Container—Thecontainerinwhichthesampleistobe
D5 Test Method for Penetration of Bituminous Materials
tested shall be a flat-bottom, cylindrical seamless tin box,
approximately 70 mm in diameter and 45 mm in depth.
1
This test method is under the jurisdiction of ASTM Committee D04 on Road NOTE 1—Containers known in the pharmaceutical industry as seamless
and Paving Materials and is the direct responsibility of Subcommittee D04.46 on
“ointment boxes” may be obtained in dimensions conforming to the above
Durability and Distillation Tests.
requirements.
Current edition approved June 1, 2014. Published June 2014. Originally
5.1.2 Heating Bath—The heating bath shall be a cast-iron
approved in 1926. Last previous edition approved in 2008 as D243 – 08. DOI:
10.1520/D0243_D0243M-14.
air bath, or equivalent, permitting the immersion of the
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
container to a depth of 32 6 5 mm through an opening 3 6 2
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
mm larger in diameter than the container. It shall support the
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. container 6 6 2 mm above the hot plate, and with at least 6.4
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D243/D243M−14
greater than the immersion depth. The PRT system (probe and
readout)shallbestandardizedinaccordancewithTestMethods
E644.
5.1.5 A balance, readable to 0.01 g,
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D243 − 08 D243/D243M − 14
Standard Test Method for
1
Residue of Specified Penetration
This standard is issued under the fixed designation D243;D243/D243M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method is used to thermally reduce cutback asphalt, a road oil or a semisolid asphalt, having a penetration greater
than 100, to a residue of specified penetration. It is primarily used with slow-curing cutback asphalt as specified in Specification
D2026.
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as the standard. The inch-pound units
given in parentheses are for information only.values stated in each system may not be exact equivalents; therefore, each system
shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency (EPA) and many state
agencies as a hazardous material that can cause central nervous system, kidney and liver damage. Mercury, or its vapor, may be
hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products.
See the applicable product Material Safety Data Sheet (MSDS) for details and EPA’s website—http://www.epa.gov/mercury/
faq.htm—forwebsite—http://www.epa.gov/mercury/—for additional information. Users should be aware that selling mercury,
mercury-containing products, or both, into your state may be prohibited by state law.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.Specific precautionary statements are given in Note 2.
2. Referenced Documents
2
2.1 ASTM Standards:
D5 Test Method for Penetration of Bituminous Materials
D2026 Specification for Cutback Asphalt (Slow-Curing Type)
E1 Specification for ASTM Liquid-in-Glass Thermometers
E77 Test Method for Inspection and Verification of Thermometers
E220 Test Method for Calibration of Thermocouples By Comparison Techniques
E644 Test Methods for Testing Industrial Resistance Thermometers
E1137/E1137M Specification for Industrial Platinum Resistance Thermometers
3. Summary of Test Method
3.1 The material to be tested is rapidly heated to 249°C (480°F)[480°F] and maintained at 249°249 to 260°C (480°[480 to
500°F)500°F] during evaporation of the volatiles. Penetration of the residue is determined and if not within the specified limits,
the evaporation procedure is repeated. Change in sample mass is used to calculate the percentage of residue having the specified
penetration.
4. Significance and Use
4.1 This test method is used to determine the percentage of residue having a specified penetration at 100 g/5 s at 25°C
(77°F).[77°F]. This test method provides a residue for quality control or for use in other tests as desired.
1
This test method is under the jurisdiction of ASTM Committee D04 on Road and Paving Materials and is the direct responsibility of Subcommittee D04.46 on Durability
and Distillation Tests.
Current edition approved July 15, 2008June 1, 2014. Published August 2008June 2014. Originally approved in 1926. Last previous edition approved in 19972008 as
D243D243 – 08.–97. DOI: 10.1520/D0243-08.10.1520/D0243_D0243M-14.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D243/D243M − 14
5. Apparatus
5.1 The apparatus shall consist of a container, heating bath, hot plate, and thermometric device, with necessary accessory
apparatus as follows:
5.1.1 Container—The container in which the sample is to be tested shall be a flat-bottom, cylindrical seamless tin box,
approximately 70 mm in diameter and 45 mm in depth.
NOTE 1—Containers known in the pharmaceutical industry a
...

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1.1 This specification2 covers asphalt binders graded by performance. Grading designations are related to the LTPPBind Online calculated maximum pavement design temperature, the minimum pavement design temperature, and the traffic loading.
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1.2 This specification incorporates Test Method D7405 for determining non-recoverable creep compliance, Jnr. “S,” “H,” “V,” or “E” designations must be specified for standard, heavy, very heavy, and extremely heavy traffic loading, respectively.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.
Note 2: A guidance document for specifying bodies using R % for elastic properties is under development.
Note 3: For asphalt binders graded by penetration at 25 °C, see Specification D946/D946M. For asphalt binders graded by viscosity at 60 °C, see Specification D3381/D3381M. For performance-graded asphalt binder, see Specification D6373.
Note 4: AASHTO R 29 provides non-mandatory information for determining the performance grade of an asphalt binder.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D6373-23(Specification)
Standard Specification for Performance-Graded Asphalt Binder

ABSTRACT
This specification covers asphalt binders graded by performance. Grading designations are related to the average seven-day maximum pavement design temperature, and minimum pavement design temperature. Asphalt binder shall be prepared by the refining of crude petroleum by suitable methods, with or without the addition of modifiers, which may be any organic material of suitable manufacture that is used in virgin or recycled condition, and that is dissolved, dispersed or reacted in asphalt cement to enhance its performance. This specification incorporates an aid for determining the critical low cracking temperature using a combination of test procedures.
SCOPE
1.1 This specification2 covers asphalt binders graded by performance. Grading designations are related to the LTPPBind Online calculated maximum pavement design temperature and the minimum pavement design temperature. This specification contains Tables 1 and 2. Table 2 incorporates Practice D6816 for determining the critical low cracking temperature using a combination of Test Method D6648 and Test Method D6723 test procedures. If no table is specified, the default is Table 1.
Note 1: For more information on LTPPBind Online, see https://infopave.fhwa.dot.gov/Tools/LTPPBindOnline accessed May 23, 2023.
Note 2: For asphalt cements graded by penetration at 25 °C, see Specification D946/D946M. For asphalt cements graded by viscosity at 60 °C, see Specification D3381/D3381M.
Note 3: AASHTO R 29 provides non-mandatory information for determining the performance grade of an asphalt binder.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Technical specification
    5 pages
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  • Technical specification
    5 pages
    English language
    sale 15% off