ISO 12743:2018
(Main)Copper, lead, zinc and nickel concentrates — Sampling procedures for determination of metal and moisture content
Copper, lead, zinc and nickel concentrates — Sampling procedures for determination of metal and moisture content
This document sets out the basic methods for sampling copper, lead, zinc and nickel concentrates from moving streams and stationary lots, including stopped-belt sampling, to provide samples for chemical analysis, physical testing and determination of moisture content, in accordance with the relevant International Standards. Where the concentrates are susceptible to significant oxidation or decomposition, a common sample that is sufficiently representative, i.e. unbiased and sufficiently precise, is used for moisture determination and chemical analysis to eliminate bias (see ISO 10251). Any large agglomerates (>10 mm) present in the primary sample are crushed prior to further sample processing. Sampling of concentrates in slurry form is specifically excluded from this document. Stopped-belt sampling is the reference method for collecting concentrate samples against which mechanical and manual-sampling procedures can be compared. Sampling from moving streams is the preferred method. Both falling-stream and cross-belt samplers are described. Sampling from stationary lots is used only where sampling from moving streams is not possible. The procedures described in this document, for sampling from stationary lots, only minimize some of the systematic sampling errors.
Concentrés de cuivre, de plomb, de zinc et de nickel — Procédures d'échantillonnage pour la détermination de la teneur en métal et de l'humidité
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Standards Content (Sample)
INTERNATIONAL ISO
STANDARD 12743
Third edition
2018-06
Copper, lead, zinc and nickel
concentrates — Sampling procedures
for determination of metal and
moisture content
Concentrés de cuivre, de plomb, de zinc et de nickel — Procédures
d'échantillonnage pour la détermination de la teneur en métal et de
l'humidité
Reference number
©
ISO 2018
© ISO 2018
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Contents Page
Foreword .vi
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Sampling theory . 4
4.1 General . 4
4.2 Total variance . 4
4.3 Sampling-stage method of estimating sampling and total variance . 6
4.4 Simplified method of estimating sampling and total variance . 9
4.5 Interleaved sample method of measuring total variance .10
5 Establishing a sampling scheme .12
6 Mass of increment .17
6.1 General .17
6.2 Mass of increment for falling-stream samplers .17
6.3 Mass of increment for cross-belt samplers .17
6.4 Mass of increment for manual sampling from stationary lots .17
6.4.1 Primary increments .17
6.4.2 Mass of secondary and subsequent increments .18
6.5 Mass of increment for stopped-belt reference sampling .18
7 Methods of sampling from concentrate streams .18
7.1 General .18
7.2 Mass-basis systematic sampling .18
7.2.1 General.18
7.2.2 Sampling interval .19
7.2.3 Sample cutter .19
7.2.4 Taking of primary increments .19
7.2.5 Constitution of subsamples and lot samples .19
7.2.6 Types of division .20
7.2.7 Division of increments .20
7.2.8 Division of subsamples .20
7.2.9 Division of lot samples .20
7.3 Time-basis systematic sampling .21
7.3.1 General.21
7.3.2 Sampling interval .21
7.3.3 Sample cutter .21
7.3.4 Taking of primary increments .22
7.3.5 Constitution of subsamples and lot samples .22
7.3.6 Types of division .22
7.3.7 Division of increments and subsamples .22
7.3.8 Division of lot samples .22
7.4 Stratified random sampling .22
7.4.1 Fixed mass intervals .22
7.4.2 Fixed time intervals .23
8 Mechanical sampling of concentrate streams .23
8.1 General .23
8.2 Design of the sampling system .23
8.2.1 Safety of operators .23
8.2.2 Location of sample cutters .23
8.2.3 Provision for interleaved sampling .23
8.2.4 Provision for stratified random sampling .24
8.2.5 Checking precision and bias.24
8.2.6 Avoiding bias .24
8.2.7 Minimizing bias .24
8.2.8 Configuration of the sampling system .24
8.3 Sample cutters .24
8.3.1 General.24
8.3.2 Design criteria .25
8.3.3 Cutter speed .26
8.4 Mass of increments.26
8.5 Number of increments .27
8.6 Sampling interval .27
8.7 Routine checking .27
9 Manual sampling of concentrate streams .28
9.1 General .28
9.2 Choosing the sampling location .28
9.3 Sampling implements .28
9.4 Mass of increments.28
9.5 Number of increments .28
9.6 Sampling interval .28
9.7 Sampling procedures .29
9.7.1 General.29
9.7.2 Full stream cut from a falling stream .29
9.7.3 Partial stream cuts from a falling stream .29
9.7.4 Sampling from moving conveyor belts .30
10 Stopped-belt reference sampling .30
11 Sampling from grabs .
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