ASTM C1031-11(2022)
(Specification)Standard Specification for Nuclear-Grade Aluminum Oxide Powder
Standard Specification for Nuclear-Grade Aluminum Oxide Powder
ABSTRACT
This specification provides the chemical and physical properties and requirements for nuclear-grade aluminum oxide powder intended for fabrication into shapes for nuclear applications. The materials shall conform to physical requirements as to particle size distribution, and specific surface area, and chemical requirements as to loss-on-ignition, and total and elemental concentrations of all impurities. Impurities may include silicaon, iron-chromium-nickel, magnesium, sodium, calcium, hafnium, fluorine, fluorine-chlorine-iodine-bromine, gadolinium, samarium, europium, and dysprosium.
SCOPE
1.1 This specification provides the chemical and physical requirements for nuclear-grade aluminum oxide powder intended for fabrication into shapes for nuclear applications. Two specific uses for which this powder is intended are Al2O3 pellets and Al2O3 − B4C composite pellets for use as thermal insulator or burnable neutron absorbers, respectively.
1.2 The material described herein shall be particulate in nature.
1.3 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
General Information
- Status
- Published
- Publication Date
- 30-Jun-2022
- Technical Committee
- C26 - Nuclear Fuel Cycle
- Drafting Committee
- C26.03 - Neutron Absorber Materials Specifications
Relations
- Effective Date
- 01-Jan-2024
- Effective Date
- 01-Feb-2019
- Effective Date
- 15-Jun-2014
- Effective Date
- 15-Jan-2014
- Effective Date
- 01-Jun-2013
- Effective Date
- 01-May-2013
- Effective Date
- 01-Jan-2013
- Effective Date
- 01-Nov-2010
- Effective Date
- 01-Oct-2010
- Effective Date
- 01-Aug-2010
- Effective Date
- 01-Feb-2010
- Effective Date
- 15-Feb-2009
- Effective Date
- 15-Sep-2008
- Effective Date
- 01-Jul-2007
- Effective Date
- 01-Jun-2004
Overview
ASTM C1031-11(2022): Standard Specification for Nuclear-Grade Aluminum Oxide Powder specifies the requirements for aluminum oxide (Al₂O₃) powder used in nuclear applications. Developed by ASTM International, this standard outlines both chemical and physical properties essential for nuclear-grade materials, ensuring the suitability and safety of aluminum oxide powders intended for fabrication into various shapes.
This specification addresses the needs of nuclear facilities and manufacturers, particularly those involved in producing Al₂O₃ pellets for thermal insulation or Al₂O₃–B₄C composite pellets as burnable neutron absorbers. Adherence to this standard ensures high-quality nuclear-grade aluminum oxide powder with controlled particle size and purity, meeting international safety and quality benchmarks.
Key Topics
Chemical Composition
- Defines maximum allowable concentrations for impurities such as silicon, iron-chromium-nickel, magnesium, sodium, calcium, hafnium, halides (fluorine, chlorine, iodine, bromine), and rare earth elements (gadolinium, samarium, europium, dysprosium).
- The total concentration of all measured impurities must not exceed 4.0 weight percent.
- Loss-on-ignition testing requirements are agreed upon between the buyer and seller.
Physical Properties
- Specifies particulate nature and particle size distribution, with the mean particle size not exceeding 6 µm.
- Requirements for specific surface area are mutually determined between buyer and seller.
Packaging and Marking
- Material must be packaged in sealed containers to prevent contamination, with comprehensive marking that includes product identification, lot number, order details, and seller information.
Sampling and Quality Control
- Stipulates rigorous sampling plans and inspection routines.
- Sellers must provide certificates of analysis for each lot, verifying compliance with the standard.
Quality Assurance
- References regulations like the Code of Federal Regulations Title 10, Part 50, and ANSI/ASME NQA-1 for additional quality assurance guidelines.
Applications
Nuclear Fuel Fabrication
- Manufactures Al₂O₃ pellets used as thermal insulators in nuclear reactors.
- Produces Al₂O₃–B₄C composite pellets, which function as burnable neutron absorbers, controlling reactivity in nuclear cores.
Advanced Reactor Systems
- Supports next-generation nuclear technology requiring precise material control.
Nuclear Facility Maintenance and Upgrades
- Used in the refurbishment of reactor components where new or replacement shapes are fabricated.
By setting rigorous chemical and physical criteria, ASTM C1031-11(2022) ensures aluminum oxide powders are robust, consistent, and safe for use in sensitive nuclear applications. This standard helps maintain high levels of nuclear facility performance, reliability, and compliance with international safety directives.
Related Standards
- ASTM C809 – Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Aluminum Oxide and Aluminum Oxide-Boron Carbide Composite Pellets.
- ASTM C859 – Terminology Relating to Nuclear Materials.
- ASTM E105 – Guide for Probability Sampling of Materials.
- ANSI/ASME NQA-1 – Quality Assurance Requirements for Nuclear Facility Applications.
- CFR Title 10, Part 50 – US Code of Federal Regulations regarding domestic licensing of production and utilization nuclear facilities.
For organizations involved in nuclear fuel production or research, following ASTM C1031-11(2022) is essential to meet industry standards for nuclear-grade aluminum oxide powder. Ensuring conformity supports quality control, regulatory compliance, and operational excellence in nuclear environments.
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Frequently Asked Questions
ASTM C1031-11(2022) is a technical specification published by ASTM International. Its full title is "Standard Specification for Nuclear-Grade Aluminum Oxide Powder". This standard covers: ABSTRACT This specification provides the chemical and physical properties and requirements for nuclear-grade aluminum oxide powder intended for fabrication into shapes for nuclear applications. The materials shall conform to physical requirements as to particle size distribution, and specific surface area, and chemical requirements as to loss-on-ignition, and total and elemental concentrations of all impurities. Impurities may include silicaon, iron-chromium-nickel, magnesium, sodium, calcium, hafnium, fluorine, fluorine-chlorine-iodine-bromine, gadolinium, samarium, europium, and dysprosium. SCOPE 1.1 This specification provides the chemical and physical requirements for nuclear-grade aluminum oxide powder intended for fabrication into shapes for nuclear applications. Two specific uses for which this powder is intended are Al2O3 pellets and Al2O3 − B4C composite pellets for use as thermal insulator or burnable neutron absorbers, respectively. 1.2 The material described herein shall be particulate in nature. 1.3 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
ABSTRACT This specification provides the chemical and physical properties and requirements for nuclear-grade aluminum oxide powder intended for fabrication into shapes for nuclear applications. The materials shall conform to physical requirements as to particle size distribution, and specific surface area, and chemical requirements as to loss-on-ignition, and total and elemental concentrations of all impurities. Impurities may include silicaon, iron-chromium-nickel, magnesium, sodium, calcium, hafnium, fluorine, fluorine-chlorine-iodine-bromine, gadolinium, samarium, europium, and dysprosium. SCOPE 1.1 This specification provides the chemical and physical requirements for nuclear-grade aluminum oxide powder intended for fabrication into shapes for nuclear applications. Two specific uses for which this powder is intended are Al2O3 pellets and Al2O3 − B4C composite pellets for use as thermal insulator or burnable neutron absorbers, respectively. 1.2 The material described herein shall be particulate in nature. 1.3 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
ASTM C1031-11(2022) is classified under the following ICS (International Classification for Standards) categories: 27.120.30 - Fissile materials and nuclear fuel technology; 71.060.20 - Oxides. The ICS classification helps identify the subject area and facilitates finding related standards.
ASTM C1031-11(2022) has the following relationships with other standards: It is inter standard links to ASTM C859-24, ASTM C809-19, ASTM C859-14a, ASTM C859-14, ASTM C859-13a, ASTM C859-13, ASTM C809-13, ASTM C859-10b, ASTM E105-10, ASTM C859-10a, ASTM C859-10, ASTM C859-09, ASTM C859-08, ASTM C809-94(2007), ASTM E105-04. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.
ASTM C1031-11(2022) is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.
Standards Content (Sample)
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation:C1031 −11 (Reapproved 2022)
Standard Specification for
Nuclear-Grade Aluminum Oxide Powder
This standard is issued under the fixed designation C1031; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 2.3 U.S. Government Document:
Code of Federal Regulations, Title 10,Part 50–Energy
1.1 This specification provides the chemical and physical
(10CFR 50), Domestic Licensing of Production and Uti-
requirements for nuclear-grade aluminum oxide powder in-
lization Facilities
tendedforfabricationintoshapesfornuclearapplications.Two
specific uses for which this powder is intended are Al O
2 3
3. Terminology
pellets and Al O −B C composite pellets for use as thermal
2 3 4
3.1 Definitions of Terms Specific to This Standard:
insulator or burnable neutron absorbers, respectively.
3.1.1 Terms shall be defined in accordance with Terminol-
1.2 The material described herein shall be particulate in
ogy C859 except for the following:
nature.
3.1.2 buyer—organization issuing the purchase order.
1.3 Units—The values stated in SI units are to be regarded
3.1.3 powder lot—that quantity of aluminum oxide powder
asstandard.Nootherunitsofmeasurementareincludedinthis
madeupofpowderfromoneormoresources,blendedtogether
standard.
and homogenized such that samples taken in accordance with
theproceduresinSection8canbeconsideredasrepresentative
1.4 This international standard was developed in accor-
of the entire quantity.
dance with internationally recognized principles on standard-
ization established in the Decision on Principles for the
3.1.4 seller—aluminum oxide manufacturer.
Development of International Standards, Guides and Recom-
4. Ordering Information
mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee.
4.1 Thebuyershallspecifythefollowinginformationonthe
order:
2. Referenced Documents
4.1.1 Quantity (weight of delivered product),
4.1.2 Lot size (allowable range),
2.1 ASTM Standards:
4.1.3 Sample requirements, and
C809Test Methods for Chemical, Mass Spectrometric, and
4.1.4 Additional requirements.
Spectrochemical Analysis of Nuclear-Grade Aluminum
Oxide and AluminumOxide-Boron Carbide Composite
5. Chemical Composition
Pellets
5.1 The powder shall conform to the following chemical
C859Terminology Relating to Nuclear Materials
requirements (see Methods C809):
E105Guide for Probability Sampling of Materials
Element Weight %, max
2.2 ANSI Standard:
Silicon 2.0
ANSI/ASME NQA-1Quality Assurance Requirements for
Iron-Chromium-Nickel 0.6
Magnesium 1.0
Nuclear Facility Applications
Sodium 0.2
Calcium 0.3
Hafnium 200 µg/g Al O
2 3
Fluorine 50 µg/g Al O
2 3
This specification is under the jurisdiction of ASTM Committee C26 on
Fluorine-Chlorine-Iodine-Bromine 100 µg/g Al O
2 3
Nuclear Fuel Cycle and is the direct responsibility of Subcommittee C26.03 on
Gadolinium 100 µg/g Al O
2 3
Neutron Absorber Materials Specifications.
Samarium 100 µg/g Al O
2 3
CurrenteditionapprovedJuly1,2022.PublishedJuly2022.Originallyapproved
Europium 100 µg/g Al O
2 3
in 1984. Last previous edition approved in 2016 as C1031–11(2016). DOI:
Dysprosium 200 µg/g Al O
2 3
10.1520/C1031-11R22.
5.2 The impurities listed in 5.1, and any other identified
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
impurityexceeding1.0weight%andthetotalconcentrationof
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website.
3 4
Available fromAmerican National Standards Institute (ANSI), 25 W. 43rd St., AvailablefromU.S.GovernmentPrintingOfficeSuperintendentofDocuments,
4th Floor, New York, NY 10036. 732 N. Capitol St., NW, Mail Stop: SDE, Washington, D.C., 20401.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
C1031−11 (2022)
all impurities, shall be reported. The total of all measured 9.1.2 Individual and total impurities,
impurities shall not exceed 4.0 weight%. 9.1.3 Particle size distribution and mean value,
9.1.4 Specific surface area, and
5.3 Loss-on-Ignition—The test method and acceptance lim-
9.1.5
...




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