Standard Specification for Emulsified Coal-Tar Pitch (Mineral Colloid Type)

ABSTRACT
This specification describes the test methods for and physical requirements of mineral-colloid-stabilized, emulsified coal-tar pitch suitable for use as a weather-protective and aliphatic-solvent resistant coating over bituminous pavements of airports, parking areas, and driveways. The emulsion shall be made using tars having viscosities of RT-11 or higher, and the mineral filler (mineral colloids) shall consist of finely ground clay, silica, or other inert inorganic materials. And when specified, the emulsion shall be fortified with antifreeze. The properties for which coal-tar pitches shall be appropriately tested on and accordingly adhere to are: wet film continuity; freezing resistance; density; volatile matter content; residue by evaporation; volatilization resistance and residue weight loss; solubility of residue in CS2; ash content of residue; flammability; drying time and firm set; heat resistance; resistance to kerosene and water; and impact resistance before and after accelerated weathering.
SCOPE
1.1 This specification covers mineral-colloid-stabilized, emulsified coal-tar pitch suitable for use as a weather-protective and aliphatic-solvent resistant coating over bituminous pavements of airports, parking areas, and driveways.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.  
1.3 The following precautionary caveat pertains only to the test method portion, Section 6, of this specification:  This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
30-Sep-2018

Relations

Effective Date
01-Oct-2018
Effective Date
01-Dec-2023
Effective Date
01-Oct-2018
Effective Date
01-May-2018
Effective Date
01-Jun-2016
Effective Date
01-Jun-2015
Effective Date
01-Jun-2014
Effective Date
15-Nov-2013
Effective Date
15-Nov-2013
Effective Date
15-Jun-2013
Effective Date
01-May-2013
Effective Date
01-Dec-2011
Effective Date
01-Jun-2009
Effective Date
01-Sep-2008
Effective Date
01-Nov-2007

Overview

ASTM D3320/D3320M-18 - Standard Specification for Emulsified Coal-Tar Pitch (Mineral Colloid Type) establishes requirements for mineral-colloid-stabilized, emulsified coal-tar pitch used as a weather-protective and solvent-resistant coating. This standard is widely recognized for promoting product consistency and quality in surface protection for bituminous pavements at airports, parking areas, and driveways. The specification covers material composition, physical and chemical properties, application methods, and testing criteria for emulsified coal-tar pitch, ensuring durable performance in demanding environments.

Key Topics

  • Product Requirements: Only tars with viscosities of RT-11 or higher are allowed, and mineral fillers must be finely ground inorganic materials such as clay or silica. The emulsion may be fortified with antifreeze when specified.
  • Physical Properties: The coal-tar pitch must meet detailed requirements for wet film continuity, freezing resistance, density, volatile matter content, residue by evaporation, resistance to volatilization, solubility, ash content, flammability, drying time, heat resistance, resistance to kerosene and water, and impact resistance, both before and after accelerated weathering.
  • Testing and Conformity: Methods for sampling, testing, inspection, certification, and retesting are prescribed to ensure the material's quality and conformity to the specification.
  • Safety and Handling: The standard reminds users of the need to establish proper safety, health, and environmental practices and compliance with relevant regulations during use and application.

Applications

ASTM D3320/D3320M-18 is essential for construction and maintenance projects requiring high-performance protective surface treatments for bituminous pavements. Typical applications include:

  • Airport Pavements: Offers superior protection against weather and aliphatic solvents commonly found in aviation environments.
  • Parking Areas and Driveways: Extends pavement life by providing resistance to fuel, oil, water, and temperature extremes.
  • Industrial and Commercial Surfaces: Suitable in settings where chemical spills and harsh weather are concerns, as the emulsion resists both water and a range of solvents.

The standard guarantees that applied coatings meet stringent durability and safety benchmarks. The product is designed for convenient application by brush, squeegee, roller, or spray on properly prepared, non-diluted surfaces.

Related Standards

Professionals working with ASTM D3320/D3320M-18 may also reference the following standards for broader compliance and best practices:

  • ASTM D140/D140M – Practice for Sampling Asphalt Materials
  • ASTM D490 – Specification for Road Tar
  • ASTM D2939 – Test Methods for Emulsified Bitumens Used as Protective Coatings (withdrawn)
  • ASTM D3699 – Specification for Kerosine
  • ASTM D529 – Practice for Enclosed Carbon-Arc Exposures of Bituminous Materials (withdrawn)
  • Federal Specification VV-K-211 – Kerosene

These related standards support consistent sampling, testing, and material requirements across a wide range of bituminous and protective coating applications.


Keywords: ASTM D3320, emulsified coal-tar pitch, mineral colloid, bituminous pavement coating, airport pavement protection, solvent-resistant coating, weather-protective sealant, pavement maintenance standard.

Buy Documents

Technical specification

ASTM D3320/D3320M-18 - Standard Specification for Emulsified Coal-Tar Pitch (Mineral Colloid Type)

English language (3 pages)
sale 15% off
sale 15% off

Get Certified

Connect with accredited certification bodies for this standard

ICC Evaluation Service

Building products evaluation and certification.

ANAB United States Verified

QAI Laboratories

Building and construction product testing and certification.

ANAB United States Verified

Aboma Certification B.V.

Specialized in construction, metal, and transport sectors.

RVA Netherlands Verified

Sponsored listings

Frequently Asked Questions

ASTM D3320/D3320M-18 is a technical specification published by ASTM International. Its full title is "Standard Specification for Emulsified Coal-Tar Pitch (Mineral Colloid Type)". This standard covers: ABSTRACT This specification describes the test methods for and physical requirements of mineral-colloid-stabilized, emulsified coal-tar pitch suitable for use as a weather-protective and aliphatic-solvent resistant coating over bituminous pavements of airports, parking areas, and driveways. The emulsion shall be made using tars having viscosities of RT-11 or higher, and the mineral filler (mineral colloids) shall consist of finely ground clay, silica, or other inert inorganic materials. And when specified, the emulsion shall be fortified with antifreeze. The properties for which coal-tar pitches shall be appropriately tested on and accordingly adhere to are: wet film continuity; freezing resistance; density; volatile matter content; residue by evaporation; volatilization resistance and residue weight loss; solubility of residue in CS2; ash content of residue; flammability; drying time and firm set; heat resistance; resistance to kerosene and water; and impact resistance before and after accelerated weathering. SCOPE 1.1 This specification covers mineral-colloid-stabilized, emulsified coal-tar pitch suitable for use as a weather-protective and aliphatic-solvent resistant coating over bituminous pavements of airports, parking areas, and driveways. 1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. 1.3 The following precautionary caveat pertains only to the test method portion, Section 6, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ABSTRACT This specification describes the test methods for and physical requirements of mineral-colloid-stabilized, emulsified coal-tar pitch suitable for use as a weather-protective and aliphatic-solvent resistant coating over bituminous pavements of airports, parking areas, and driveways. The emulsion shall be made using tars having viscosities of RT-11 or higher, and the mineral filler (mineral colloids) shall consist of finely ground clay, silica, or other inert inorganic materials. And when specified, the emulsion shall be fortified with antifreeze. The properties for which coal-tar pitches shall be appropriately tested on and accordingly adhere to are: wet film continuity; freezing resistance; density; volatile matter content; residue by evaporation; volatilization resistance and residue weight loss; solubility of residue in CS2; ash content of residue; flammability; drying time and firm set; heat resistance; resistance to kerosene and water; and impact resistance before and after accelerated weathering. SCOPE 1.1 This specification covers mineral-colloid-stabilized, emulsified coal-tar pitch suitable for use as a weather-protective and aliphatic-solvent resistant coating over bituminous pavements of airports, parking areas, and driveways. 1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. 1.3 The following precautionary caveat pertains only to the test method portion, Section 6, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D3320/D3320M-18 is classified under the following ICS (International Classification for Standards) categories: 91.100.50 - Binders. Sealing materials. The ICS classification helps identify the subject area and facilitates finding related standards.

ASTM D3320/D3320M-18 has the following relationships with other standards: It is inter standard links to ASTM D3320-00(2004)e1, ASTM D140/D140M-16(2023), ASTM D3699-18a, ASTM D3699-18, ASTM D140/D140M-16, ASTM D140/D140M-15, ASTM D140/D140M-14, ASTM D3699-13b, ASTM D3699-13be1, ASTM D3699-13a, ASTM D3699-13, ASTM D490-92(2011), ASTM D140/D140M-09, ASTM D3699-08, ASTM D3699-07. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

ASTM D3320/D3320M-18 is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.

Standards Content (Sample)


This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D3320/D3320M −18
Standard Specification for
Emulsified Coal-Tar Pitch (Mineral Colloid Type)
This standard is issued under the fixed designation D3320/D3320M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope minous Materials (Withdrawn 2013)
D2939Test Methods for Emulsified Bitumens Used as
1.1 This specification covers mineral-colloid-stabilized,
Protective Coatings (Withdrawn 2012)
emulsified coal-tar pitch suitable for use as a weather-
D3699Specification for Kerosine
protective and aliphatic-solvent resistant coating over bitumi-
2.2 Federal Specification:
nous pavements of airports, parking areas, and driveways.
VV-K-211Kerosene
1.2 The values stated in either SI units or inch-pound units
are to be regarded separately as standard. The values stated in
3. Materials and Manufacture
each system may not be exact equivalents; therefore, each
3.1 Theemulsionshallbemadeusingtarshavingviscosities
system shall be used independently of the other. Combining
of RT-11 or higher. The tars shall conform to the requirements
values from the two systems may result in non-conformance
of Specification D490.
with the standard.
3.2 Mineral filler (mineral colloids) shall consist of finely
1.3 The following precautionary caveat pertains only to the
ground clay, silica, or other inert inorganic materials.
test method portion, Section 6, of this specification: This
(Warning—Bentonitic or highly expansive clays may cause
standard does not purport to address all of the safety concerns,
dryingandshrinkageproblems,whichmayaffectthedurability
if any, associated with its use. It is the responsibility of the user
of the pavement sealer.)
of this standard to establish appropriate safety, health, and
environmental practices and determine the applicability of
3.3 When specified, the emulsion shall be fortified with
regulatory limitations prior to use.
antifreeze.
1.4 This international standard was developed in accor-
dance with internationally recognized principles on standard- 4. Physical Requirements
ization established in the Decision on Principles for the
4.1 The emulsion shall be of suitable consistency for appli-
Development of International Standards, Guides and Recom-
cation by brush, squeegee, roller, or suitable spray equipment.
mendations issued by the World Trade Organization Technical
The material shall be used as received. It shall not be diluted
Barriers to Trade (TBT) Committee.
with water or thinned by heating. It shall bond firmly to
properly prepared damp or primed surfaces.
2. Referenced Documents
NOTE 1—Pavement and ambient temperature should be not less than
2.1 ASTM Standards:
7°C [45°F] at the time of application and for at least 12 h thereafter, with
no precipitation of rain, snow, and so forth, until the emulsion has dried.
D140/D140MPractice for Sampling Asphalt Materials
D490Specification for Road Tar
4.2 The product shall be of smooth, uniform consistency
D529Practice for Enclosed Carbon-Arc Exposures of Bitu-
without settlement or segregation in storage to the extent that
it cannot be readily dispersed by ordinary stirring.
4.3 The material, after stirring to homogeneity, shall be
This specification is under the jurisdiction of ASTM Committee D08 on
suitable for application by the selected method in single coats
Roofing andWaterproofing and is the direct responsibility of SubcommitteeD08.09
2 2
of approximately 0.3 to 0.4 L/m [ ⁄4to 1 gal/100 ft ] without
on Bituminous Emulsions.
appreciable drainage on inclines up to 0.8% [0.1 in./ft].
Current edition approved Oct. 1, 2018. Published November 2018. Originally
ɛ1
approved in 1974. Last previous edition approved in 2004 as D3320–00 (2004) ,
which was withdrawn in July 2013 and reinstated in October 2018. DOI:
10.1520/D3320_D3320M-18.
2 3
For referenced ASTM standards, visit the ASTM website, www.astm.org, or The last approved version of this historical standard is referenced on
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM www.astm.org.
Standards volume information, refer to the standard’s Document Summary page on Obsolete. Previously available from Standardization Documents Order Desk,
the ASTM website. Bldg. 4 Section D, 700 RobbinsAve. Philadelphia, PA19111-5094,Attn: NPODS.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D3320/D3320M − 18
4.4 The material shall conform to the physical properties 6.10 Drying Time—Test Methods D2939, Section 13 on
prescribed in Table 1 prior to fortification with antifreeze. Drying Time, except test after drying for 8 h.
6.11 Resistance to Heat—Test Methods D2939, Section 14
5. Sampling
on Resistance to Heat, 80 6 3°C [176 6 5°F] for 2 h.
5.1 Sample in accordance with Practice D140/D140M and
6.12 Resistance to Kerosine—Test Methods D2939, except
Test Methods D2939.
apply the emulsion in two coats and use kerosine in testing
applied film.
6. Test Methods
6.12.1 Apply the material in two coats using a brass mask
6.1 Wet Film Continuity—Using a spatula, spread the wet
1.6 mm [ ⁄64 in.] in thickness for the first coat and a 3.2-mm
emulsiontoathinfilmonasheetofstandard67.7-g/m [18-lb]
[ ⁄64-in.] brass mask with the same rectangular opening as the
mimeograph paper.As the emulsion is drawn out to a smear, it
first mask for the second coat, so that the cured film has a
shall show a uniformly smooth nongranular consistency, free
minimum thickness of 1.6 mm [0.06 in.]. Leave the mask for
of coarse particles.
the first coat in place during the drying period and remove it
6.2 Resistance to Freezing (when specified)—Expose a rep-
before the second mask is positioned for the final coating
resentative specimen of the emulsion to a temperature
application.
of−18°C [0°F] for 24 h; then warm the specimen
...

Questions, Comments and Discussion

Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.

Loading comments...