Standard Test Methods for Determining Bulk Density of Granular Carriers and Granular Pesticides

SIGNIFICANCE AND USE
3.1 These test methods were designed principally for clay, corncob, nut shell, paper-based or sand granular carriers, and granular pesticide products, but need not be limited to these materials. There may be more appropriate test methods for other types of granular carriers or pesticide products. The differences in the following test methods are slight, but they offer a choice of a recognized test procedure.
SCOPE
1.1 These test methods are used to determine bulk density of granular carriers and granular pesticides by measuring either free-fall bulk density (Test Method A) or loose-fill bulk density (Test Method B).  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements see Section 4.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
30-Nov-2020

Relations

Effective Date
01-Nov-2006
Effective Date
01-Jan-2001
Effective Date
01-Jan-2001

Overview

ASTM E727/E727M-08(2020) is an international standard developed by ASTM International that provides precise test methods for determining the bulk density of granular carriers and granular pesticides. It is primarily intended for use with clay, corncob, nut shell, paper-based, or sand granular materials, but is sufficiently flexible to accommodate a wide range of granular products. The standard offers recognized procedures for evaluating free-fall and loose-fill bulk density, supporting quality assurance and formulation consistency during material manufacturing and handling.

Key Topics

  • Bulk Density Measurement:
    The standard outlines two main approaches for determining bulk density:

    • Test Method A – Free-Fall Bulk Density: Measures the bulk density by filling a cylinder with granular sample via free-fall, then weighing and calculating density.
    • Test Method B – Loose-Fill Bulk Density: Involves filling a dry pint cup with material, leveling, and weighing to determine density.
  • Applicable Materials:
    Designed for granular pesticides and carriers made from clay, corncob, nut shell, sand, or paper, but it is not limited to these.

  • Measurement Units:
    Provides procedures for bulk density determination in both SI units (kg/m³) and inch-pound units (lb/ft³). Each measurement system is to be used independently to ensure compliance.

  • Safety Considerations:
    Emphasizes the need for appropriate safety, health, and environmental practices during testing, including reading product labels, preventing exposure, and using personal protective equipment.

  • Procedural Flexibility:
    Offers slight variations in methodology, allowing users to select the most appropriate, recognized procedure for their specific granular product.

Applications

  • Agricultural Chemical Production:
    Bulk density is a critical property in the formulation of granular pesticides. Accurate density measurements ensure efficient blending, packaging, transport, and application of these products.

  • Quality Control Laboratories:
    Analytical and quality assurance professionals employ these test methods to verify the consistency and conformity of granular materials to specification.

  • Material Handling and Packaging:
    Understanding bulk density informs bin design, transport logistics, and packaging requirements for granular carriers and pesticides.

  • Research and Development:
    Supports product development teams in evaluating new carrier materials or granular pesticide formulations for performance and processing characteristics.

  • Regulatory Compliance:
    Satisfies international and national requirements for bulk density data in product registration, labeling, and safety documentation.

Related Standards

  • ASTM E725 - Test Method for Sampling Granular Carriers and Granular Pesticides: Ensures representative sampling of granules for subsequent bulk density testing.

  • International Standards (WTO TBT Committee):
    Developed in line with global standardization principles, aiding mutual recognition and regulatory acceptance across borders.

  • Other Granular Material Standards:
    Various ASTM and ISO methods may exist for other types of granular materials not specifically covered by ASTM E727/E727M.


Keywords: ASTM E727, bulk density, granular pesticides, granular carriers, free-fall bulk density, loose-fill bulk density, agricultural chemicals, quality control, carrier materials, pesticide formulation, international standards

By applying ASTM E727/E727M-08(2020), organizations can achieve reliable, consistent results in measuring the bulk density of granular products, supporting process control, regulatory compliance, and product performance across the agricultural and chemical industries.

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Frequently Asked Questions

ASTM E727/E727M-08(2020) is a standard published by ASTM International. Its full title is "Standard Test Methods for Determining Bulk Density of Granular Carriers and Granular Pesticides". This standard covers: SIGNIFICANCE AND USE 3.1 These test methods were designed principally for clay, corncob, nut shell, paper-based or sand granular carriers, and granular pesticide products, but need not be limited to these materials. There may be more appropriate test methods for other types of granular carriers or pesticide products. The differences in the following test methods are slight, but they offer a choice of a recognized test procedure. SCOPE 1.1 These test methods are used to determine bulk density of granular carriers and granular pesticides by measuring either free-fall bulk density (Test Method A) or loose-fill bulk density (Test Method B). 1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements see Section 4. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE 3.1 These test methods were designed principally for clay, corncob, nut shell, paper-based or sand granular carriers, and granular pesticide products, but need not be limited to these materials. There may be more appropriate test methods for other types of granular carriers or pesticide products. The differences in the following test methods are slight, but they offer a choice of a recognized test procedure. SCOPE 1.1 These test methods are used to determine bulk density of granular carriers and granular pesticides by measuring either free-fall bulk density (Test Method A) or loose-fill bulk density (Test Method B). 1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements see Section 4. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM E727/E727M-08(2020) is classified under the following ICS (International Classification for Standards) categories: 65.100.01 - Pesticides and other agrochemicals in general. The ICS classification helps identify the subject area and facilitates finding related standards.

ASTM E727/E727M-08(2020) has the following relationships with other standards: It is inter standard links to ASTM E725-96(2006), ASTM E725-96, ASTM E725-96(2001). Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

ASTM E727/E727M-08(2020) is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.

Standards Content (Sample)


This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: E727/E727M − 08 (Reapproved 2020)
Standard Test Methods for
Determining Bulk Density of Granular Carriers and Granular
Pesticides
This standard is issued under the fixed designation E727/E727M; the number immediately following the designation indicates the year
of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval.
A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope granular pesticide products, but need not be limited to these
materials. There may be more appropriate test methods for
1.1 Thesetestmethodsareusedtodeterminebulkdensityof
other types of granular carriers or pesticide products. The
granular carriers and granular pesticides by measuring either
differences in the following test methods are slight, but they
free-fall bulk density (Test MethodA) or loose-fill bulk density
offer a choice of a recognized test procedure.
(Test Method B).
4. Hazards
1.2 The values stated in either SI units or inch-pound units
are to be regarded separately as standard. The values stated in
4.1 Before testing granular pesticides, read the precaution-
each system may not be exact equivalents; therefore, each
ary statements on the product label. Take proper precautions to
system shall be used independently of the other. Combining
prevent skin contact and inhalation of the fines and vapors.
values from the two systems may result in nonconformance
Take care to prevent contamination of the surrounding area.
with the standard.
Always wear the appropriate safety equipment and, where
indicated, wear respiratory devices approved by NIOSH for the
1.3 This standard does not purport to address all of the
product being tested.
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
5. Summary of Test Method A—Free-Fall Bulk Density
priate safety, health, and environmental practices and deter-
5.1 A tared 500-mL cylinder is filled with the granular
mine the applicability of regulatory limitations prior to use.
carrier or granular pesticide. The weight of the sample is
For specific hazard statements see Section 4.
measured and the bulk density calculated in pounds per cubic
1.4 This international standard was developed in accor-
foot or kilograms per cubic meter.
dance with internationally recognized principles on standard-
ization established in the Decision on Principles for the
6. Apparatus
Development of International Standards, Guides and Recom-
6.1 Balance, sensitivity of 1 g.
mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee.
6.2 Cylinder, graduated, capacity 500 mL. The cylinder
should be calibrated at the 500-mL mark by using 499 g water
2. Referenced Documents
at 20°C.The cylinder is cut off at the 500-mLmark and ground
2.1 ASTM Standards: smooth.
E725 Test Method for Sampling Granular Carriers and
6.3 Funnel, powder, 152 mm [6 in.] in diameter at the top,
Granular Pesticides
bottom stem opening of 25-mm [1-in.] diameter, and sides
having a slope of approximately 60°.
3. Significance and Use
6.4 Spatula, large with 51-mm [2-in.] wide blade.
3.1 These test methods were designed principally for clay,
corncob, nut shell, paper-based or sand granular carriers, and
6.5 Beaker, glass, metal, or plastic, 600-mL capacity.
6.6 Pan, metal or plastic, 203 mm [8 in.] in diameter with
These test methods are under the jurisdiction of ASTM Committee E35 on
51-mm [2-in.] sides to collect overflow of cylinder.
Pesticides, Antimicrobials, and Alternative Control Agents and are the direct
responsibility of Subcommittee E35.22 on Pesticide Formulations and Delivery
6.7 Ring Stand and Ring Clamp.
Systems.
Current edition approved Dec. 1, 2020. Published March 2021. Originally 7. Procedure
ɛ1
approved in 1980. Last previous edition approved in 2013 as E727 – 08(2013) .
7.1 Weigh the 500-mLgraduated cylinder and place it in the
DOI: 10.1520/E0727_E0727M-08R20.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or overflow pan.
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
7.2 Support the funnel on a ring which is then affixed to a
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. ring stand such that the top of the funnel is horizontal and
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
E727/E727M − 08
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