ASTM D1488-00(2018)
(Test Method)Standard Test Method for Amylaceous Matter in Adhesives
Standard Test Method for Amylaceous Matter in Adhesives
SIGNIFICANCE AND USE
5.1 This test method is used to determine if a melamine resin, a phenol, or a resorcinol adhesive contains any starch-like filler, the presence of which could affect water resistance or strength, or both.
SCOPE
1.1 This test method covers the determination of the presence or absence of amylaceous (starch-like) material in phenol-, resorcinol-, and melamine-resin adhesives.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
General Information
- Status
- Published
- Publication Date
- 31-Jul-2018
- Technical Committee
- D14 - Adhesives
- Drafting Committee
- D14.30 - Wood Adhesives
Relations
- Effective Date
- 01-Aug-2018
- Effective Date
- 01-Jul-2012
- Effective Date
- 01-May-2012
- Effective Date
- 01-Dec-2011
- Effective Date
- 01-Jan-2011
- Effective Date
- 01-Oct-2008
- Effective Date
- 15-Aug-2008
- Effective Date
- 01-Mar-2008
- Effective Date
- 01-Dec-2006
- Effective Date
- 01-Apr-2005
- Effective Date
- 01-Apr-2005
- Effective Date
- 01-Dec-2004
- Effective Date
- 01-Apr-2004
- Effective Date
- 10-May-2003
- Effective Date
- 10-Oct-2000
Overview
ASTM D1488-00(2018): Standard Test Method for Amylaceous Matter in Adhesives specifies the procedure for detecting the presence or absence of amylaceous (starch-like) materials in phenol-, resorcinol-, and melamine-resin adhesives. Developed by ASTM International, this test method is essential for quality control in adhesive manufacturing and application, as the presence of such compounds can significantly impact water resistance and structural strength of adhesive products.
This standard aligns with internationally recognized principles, as outlined by the World Trade Organization Technical Barriers to Trade (TBT) Committee, and is used by various industries and government agencies, including the U.S. Department of Defense.
Key Topics
- Significance of Detection: The main purpose of this test is to identify starch-like fillers that may compromise adhesive performance, especially regarding water resistance and bonding strength.
- Applicable Adhesives: The method applies specifically to phenol, resorcinol, and melamine-resin adhesives, which are commonly used in wood, construction, and other industrial applications.
- Test Method Summary: The procedure uses reagents such as iodine, ethyl alcohol, distilled water, and acetic acid-ethyl alcohol solution to treat adhesive samples. If amylaceous material is present, the residue reacts with the iodine solution, typically resulting in a color change.
- Sampling and Reporting: Standardized guidelines for sample collection, handling, and reporting ensure consistent and reliable testing across different batches and manufacturers.
- Safety and Compliance: Users are responsible for adhering to safety, health, and environmental protocols, as the standard does not cover specific regulatory requirements.
Applications
Implementing ASTM D1488-00(2018) provides practical benefits across several sectors:
- Quality Control in Manufacturing: Adhesive manufacturers use this standard to check batches for unwanted starch-like fillers, ensuring that products meet performance and durability requirements.
- Raw Material Verification: When sourcing adhesives, especially for structural applications, buyers can request certification of compliance with ASTM D1488 to reduce risks related to water damage or adhesive failure.
- Product Development: Formulators of phenol-, resorcinol-, and melamine-based adhesives can utilize this test method to evaluate new formulations and maintain control over filler content.
- Regulatory Compliance: Meeting ASTM D1488 is often required in procurement specifications for government or defense projects, ensuring reliability and consistency.
- Research and Testing Laboratories: Laboratories rely on this standardized method to provide third-party verification of adhesive composition for clients in various industries.
Related Standards
For a comprehensive approach to adhesive testing, the following ASTM standards and references may also be relevant:
- ASTM D907 - Terminology of Adhesives: Provides key definitions and terminology used in adhesive standards, including terms found in D1488.
- Other ASTM Adhesive Test Methods: Explore related standards for performance, durability, and environmental resistance of adhesives.
- World Trade Organization TBT Committee Guidelines: International principles for standard development, ensuring ASTM D1488's global applicability.
Organizations can refer to these related documents to ensure best practices in adhesive evaluation and to meet international quality benchmarks.
Keywords: amylaceous matter, starch-like filler, adhesive testing, phenol adhesive, resorcinol adhesive, melamine adhesive, ASTM D1488, iodine test, adhesive quality control, water resistance, industrial adhesives
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Frequently Asked Questions
ASTM D1488-00(2018) is a standard published by ASTM International. Its full title is "Standard Test Method for Amylaceous Matter in Adhesives". This standard covers: SIGNIFICANCE AND USE 5.1 This test method is used to determine if a melamine resin, a phenol, or a resorcinol adhesive contains any starch-like filler, the presence of which could affect water resistance or strength, or both. SCOPE 1.1 This test method covers the determination of the presence or absence of amylaceous (starch-like) material in phenol-, resorcinol-, and melamine-resin adhesives. 1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
SIGNIFICANCE AND USE 5.1 This test method is used to determine if a melamine resin, a phenol, or a resorcinol adhesive contains any starch-like filler, the presence of which could affect water resistance or strength, or both. SCOPE 1.1 This test method covers the determination of the presence or absence of amylaceous (starch-like) material in phenol-, resorcinol-, and melamine-resin adhesives. 1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
ASTM D1488-00(2018) is classified under the following ICS (International Classification for Standards) categories: 83.180 - Adhesives. The ICS classification helps identify the subject area and facilitates finding related standards.
ASTM D1488-00(2018) has the following relationships with other standards: It is inter standard links to ASTM D1488-00(2013), ASTM D907-12a, ASTM D907-12, ASTM D907-11a, ASTM D907-11, ASTM D907-08b, ASTM D907-08a, ASTM D907-08, ASTM D907-06, ASTM D907-05e1, ASTM D907-05, ASTM D907-04a, ASTM D907-04, ASTM D907-03, ASTM D907-00. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.
ASTM D1488-00(2018) is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.
Standards Content (Sample)
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D1488 − 00 (Reapproved 2018)
Standard Test Method for
Amylaceous Matter in Adhesives
This standard is issued under the fixed designation D1488; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope 5. Significance and Use
1.1 This test method covers the determination of the pres- 5.1 This test method is used to determine if a melamine
ence or absence of amylaceous (starch-like) material in resin, a phenol, or a resorcinol adhesive contains any starch-
phenol-, resorcinol-, and melamine-resin adhesives. like filler, the presence of which could affect water resistance
or strength, or both.
1.2 The values stated in SI units are to be regarded as the
standard. The values given in parentheses are for information
6. Reagents
only.
6.1 Iodine Test Solution—Add 5 g (0.18 oz) of iodine and 5
1.3 This standard does not purport to address all of the
g of potassium iodide to 100 mL (3 oz) of distilled water.
safety concerns, if any, associated with its use. It is the
6.2 Acetic Acid—Ethyl Alcohol Solution—Add 20 parts of
responsibility of the user of this standard to establish appro-
glacial acetic acid and 20 parts of 95 % ethyl alcohol to 60
priate safety, health, and environmental practices and deter-
parts of distilled water by volume.
mine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accor-
7. Sampling
dance with internationally recognized principles on standard-
7.1 Except in special cases, take a composite of the sample
ization established in the Decision on Principles for the
of the adhesive when possible, from three or more separate
Development of International Standards, Guides and Recom-
containers, chosen at random. Also, take samples from con-
mendations issued by the World Trade Organization Technical
tainers that appear to be nonrepresentative, and test such
Barriers to Trade (TBT) Committee.
samples separately. Before a sample is taken, thoroughly mix
the contents of the container if there is a tendency for the
2. Referenced Documents
materials to separate. Place the samples immediately in airtight
2.1 ASTM Standards:
containers and transport to the testing laboratory in these
D907 Terminology of Adhesives
containers.Take precautions to reduce evaporation or drying to
a minimum.
3. Terminology
3.1 Definitions—Many terms in this test method are defined
8. Procedure
in Terminology D907.
8.1 Phenol and Resorcinol Adhesives—Weigh 0.5 g (0.018
oz) of thoroughly mixed adhesive into a small-diameter test
4. Summary of Test Method
tube. Add 5 mL (0.15 oz) of 95 % ethyl alcohol. Shake
4.1 A reagent solution is added to the adhesive in question
thoroughly, allow the insoluble matter to settle, and decant the
which causes any starch-like material to become insoluble.The
supernatant liquid. Re
...
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